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Determination of impurities in high-purity germanium dioxide using atomic emission spectrometry
Authors:T. A. Chanysheva  I. R. Shelpakova  A. I. Saprykin
Affiliation:1.Nikolaev Institute of Inorganic Chemistry, Siberian Branch,Russian Academy of Sciences,Novosibirsk,Russia
Abstract:A technique for the determination of the impurity composition of soluble germanium dioxide and one containing up to 0.1% insoluble in 12 M HCl is described. The technique offers the possibility to control the content of 31 impurities simultaneously after preconcentration with detection limits of about 10−6 to 10−8 wt % and with an intralaboratory precision not exceeding 20 rel. %.
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