Determination of impurities in high-purity germanium dioxide using atomic emission spectrometry |
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Authors: | T. A. Chanysheva I. R. Shelpakova A. I. Saprykin |
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Affiliation: | 1.Nikolaev Institute of Inorganic Chemistry, Siberian Branch,Russian Academy of Sciences,Novosibirsk,Russia |
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Abstract: | A technique for the determination of the impurity composition of soluble germanium dioxide and one containing up to 0.1% insoluble in 12 M HCl is described. The technique offers the possibility to control the content of 31 impurities simultaneously after preconcentration with detection limits of about 10−6 to 10−8 wt % and with an intralaboratory precision not exceeding 20 rel. %. |
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