| 荧光增白剂OB—1合成工艺改进 |
| |
| 引用本文： | 易兵,林原斌. 荧光增白剂OB—1合成工艺改进[J]. 印染助剂, 2001, 18(2): 7-9 |
| |
| 作者姓名： | 易兵 林原斌 |
| |
| 作者单位： | 1. 湖南工程学院化学系,
2. 湘潭大学化学系, |
| |
| 摘 要： | 以对甲苯甲腈为原料，经氯化、环化、缩合三步反应合成了荧光增白剂双苯并恶唑二七乙烯（OB-1），通过对化合物的元素分析、红外光谱以及在DMF中紫外吸收光谱的测定，确定了目标分子，经HPLC测定，产品纯度大于99%。
|
| 关 键 词： | 荧光增白剂 双苯并恶唑二苯乙烯 合成工艺 改进 |
| 文章编号： | 1004-0439(2001)02-0007-03 |
| 修稿时间： | 2000-11-06 |
MODIFICATION OF SYNTHETIC PROCESS OF FLUORESCENT BLEACHING AGENT OB-1 |
| |
| YI Bing,LIN Yuan_bin. MODIFICATION OF SYNTHETIC PROCESS OF FLUORESCENT BLEACHING AGENT OB-1[J]. Textile Auxiliaries, 2001, 18(2): 7-9 |
| |
| Authors: | YI Bing LIN Yuan_bin |
| |
| Affiliation: | YI Bing1,LIN Yuan_bin2 |
| |
| Abstract: | With p-methylbenzonitrile as starting material, the fluorescent bleaching agent bisbenzoxazole diphenylethene (OB-1) was synthesized by chlorination, cyclization and condensation. The objective molecule was determined through testing the compound with elementary analysis, IR spectrum and ultra-violet absorption spectrometry in DMF. HPLC analysis proved that purity of the product was more than 99%. |
| |
| Keywords: | fluorescent bleaching agent bisbenzoxazole diphenylethene synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
