| 色谱法测定藿香正气水中乙醇含量 |
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| 引用本文： | 张俊花,赵倩,张洪林.色谱法测定藿香正气水中乙醇含量[J].化学与粘合,2011,33(2):73-74. |
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| 作者姓名： | 张俊花 赵倩 张洪林 |
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| 作者单位： | 辽宁石油化工大学环境与生物工程学院,辽宁抚顺,113001 |
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| 摘 要： | 用毛细管柱分离制剂中的乙醇,并以正丙醇为内标测定其含量.方法:色谱柱为毛细管柱zebron ZB-50(30m×0.32mm×0.25m);氮气为载气,柱前压0.4MPa;分流比为30:1;进样口温度为220℃,柱温45℃;FID检测器,温度为250℃;进样量1μL;正丙醇为内标物.结果:在该色谱条件下,藿香正气水中乙...
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| 关 键 词： | 藿香正气水 乙醇 气相色谱 |
Determination of Ethanol Content in Huoxiang Zhengqi Solution by Chromatography |
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| ZHANG Jun-Hua,ZHAO Qian,ZHANG Hong-Lin.Determination of Ethanol Content in Huoxiang Zhengqi Solution by Chromatography[J].Chemistry and Adhesion,2011,33(2):73-74. |
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| Authors: | ZHANG Jun-Hua ZHAO Qian ZHANG Hong-Lin |
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| Affiliation: | (College of Environmental and Biological Engineering, Liooning University of Petroleum ＆ Chemicd Technology, Fushun 113001, China) |
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| Abstract: | The ethanol in medicament was separated by capillary column, and its content was determined with using n-propanol as the internal standard. The capillary column zebron ZB-50 （30m×0.32mm×0.25m） was employed in this experiment, and the nitrogen and n-propanol was used as carrier gas and internal standard concentration, respectively. The pre-column pressure was 0.4MPa, the split ratio was 30：1, the inlet temperature was 220℃, the column temperature was 45℃, the FID detector was used at 250℃ and the injection volume was IμL. The results showed that under these conditions, the ethanol and internal standard in the Huoxiang Zhengqi solution was well separated. The linear relation was good in the range （r= 0.9995, n=7）, the average recovery rate was 97.0%. This chromatography method was high column efficiency, simple and fast and reproducible. |
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| Keywords: | Huoxiang Zhengqi solution ethanol GC |
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