| 镧改性磷酸铝介孔分子筛的合成及表征 |
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| 引用本文： | 李茂民,丛健,赵延良,宋伟明.镧改性磷酸铝介孔分子筛的合成及表征[J].化工时刊,2011,25(12):17-19. |
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| 作者姓名： | 李茂民 丛健 赵延良 宋伟明 |
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| 作者单位： | 齐齐哈尔大学,化学与化工学院 黑龙江齐齐哈尔,161006 |
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| 摘 要： | 以十八胺为模板剂,导向剂法合成磷酸铝镧介孔分子筛..采用电感耦合等离子体质谱(ICP-MS)、红外光谱(FT-IR)、N2吸附-脱附、NH3程序升温脱附(NH3-TPD)、小角度X射线衍射分析(XRD)等方法对所得样品的组成、结构和性质进行了表征.结果表明,镧修饰磷酸铝介孔分子筛与修饰前相比,比表面积略有降低,酸量和酸...
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| 关 键 词： | 磷酸铝镧分子筛 导向剂 合成 表征 |
The Synthesis and Characterization of Mesoporous Aluminophosphate Molecular Sieves Modified by La |
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| Li Maomin,Cong Jian,Zhao Yanliang,Song Weiming.The Synthesis and Characterization of Mesoporous Aluminophosphate Molecular Sieves Modified by La[J].Chemical Industry Times,2011,25(12):17-19. |
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| Authors: | Li Maomin Cong Jian Zhao Yanliang Song Weiming |
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| Affiliation: | Li Maomin Cong Jian Zhao Yanliang Song Weiming(College of Chemistry and Chemical Engineering, Qiqihar University,Heilongjiang Qiqihar 161006) |
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| Abstract: | Aluminophosphate mesoporous molecular sieves modified by La was synthesized by structure-director in non-water system using C18NH2 as template.The compose and structure of aluminophosphate mesoporous molecular sieves was characterized by Inductively Coupled Plasma Mass Spectrometry(ICP-MS,infrared spectroscopy(FT-IR),N2 adsorption-desorption,NH3chemisorption(NH3-TPD),XRD and so on.The results show that aluminophosphate mesoporous molecular sieve modified by La has slightly lower surface area,larger acid amount and acid strength compared with the sample unmodified. |
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| Keywords: | aluminophosphate molecular sieve structure-director synthesis characterization |
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