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溶剂热法可控合成纳米氯化亚铜
引用本文:李永生,韩腾,谢光勇,张爱清. 溶剂热法可控合成纳米氯化亚铜[J]. 应用化工, 2014, 0(12): 2135-2136,2143
作者姓名:李永生  韩腾  谢光勇  张爱清
作者单位:中南民族大学化学与材料科学学院催化材料科学国家民委-教育部重点实验室;
基金项目:国家自然科学基金(21172269);武汉市应用基础研究计划(2014010101010017);精细化工国家重点实验室开放基金(KF1207)
摘    要:
以氯化铜为铜源,甲醇、乙醇、异丙醇等为溶剂和还原剂,采用溶剂热法制备纳米氯化亚铜,探讨了温度、时间、还原剂等条件对所得氯化亚铜的形貌、粒径大小、物相组成的影响。结果表明,以乙醇、异丙醇为溶剂,在120~180℃反应24~48 h,Cu Cl纳米颗粒可在2~50 nm范围内有效调控。

关 键 词:氯化亚铜  纳米粒子  溶剂热法

Controllable synthesis of nano-cuprous chloride by solvothermal method
LI Yong-sheng;HAN Teng;XIE Guang-yong;ZHANG Ai-qing. Controllable synthesis of nano-cuprous chloride by solvothermal method[J]. Applied chemical industry, 2014, 0(12): 2135-2136,2143
Authors:LI Yong-sheng  HAN Teng  XIE Guang-yong  ZHANG Ai-qing
Affiliation:LI Yong-sheng;HAN Teng;XIE Guang-yong;ZHANG Ai-qing;Key Laboratory of Catalysis and Materials Science of the State Ethnic Affairs Commission & Ministry of Education,Hubei Province,South-Central University for Nationalities;
Abstract:
A solvothermal method has been developed to prepare cuprous chloride nanoparticles by reduc-ing copper chloride with methanol,ethanol and isopropanol as reducing agents and solvents,and the influ-ences of different reaction conditions such as temperatures,time and reducing agents upon the morpholo-gy,particle size and phase composition of the cuprous chloride were studied. The result showed that with ethanol and isopropanol as solvent,react 24~48 h at 120~180℃. The size of CuCl nanoparticles can be controlled in the range of 2~50 nm effectively.
Keywords:cuprous chloride  nanoparticle  solvothermal method
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