| 油溶性表面活性剂甘油硼酸油酸酯的合成研究 |
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| 引用本文： | 谢彩梅,龙得金,周孙进.油溶性表面活性剂甘油硼酸油酸酯的合成研究[J].广东化工,2009,36(11):40-41. |
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| 作者姓名： | 谢彩梅 龙得金 周孙进 |
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| 作者单位： | 茂名市石油化工研究所,广东,茂名,525011 |
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| 摘 要： | 以硼酸和油酸为原料采用直接酯化法合成水溶性的甘油硼酸酯，再在催化剂的作用下与油酸反应制得甘油硼酸油酸酷，设计出较佳的酸化条件：甘油硼酸酯与油酸摩尔比1：0．9，温度220℃，时间4h，催化剂甩量（脂肪酸质量分数）0．5％，酸转佬率98．5％。
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| 关 键 词： | 甘油硼酸酯 甘油硼酸油酸酯 表面活性剂 催化 合成 酯化 |
On the Synthesis of Oil-soluble Surfactant Glycerol Ester of Boric Acid Oil |
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| Xie Caimei,Long Dejing,Zhou Sunjin.On the Synthesis of Oil-soluble Surfactant Glycerol Ester of Boric Acid Oil[J].Guangdong Chemical Industry,2009,36(11):40-41. |
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| Authors: | Xie Caimei Long Dejing Zhou Sunjin |
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| Affiliation: | (Institute of Maoming Petrochemical, Maoming 525011, China) |
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| Abstract: | Water-soluble borate, obtained by direct esterification with boric acidn and oleic acid as raw materials, reacted with oleic acid under the action of a catalyst to produce glycerol boric acid borate. Better design of esterification conditions were as follows： molar ratio of glycerol borate and oleic acid 1：0.9, temperature 220 ~C, time 4 h, amount of catalyst （mass fraction of fatty acids） 0.5 %, acid conversion rate 98.5 %. |
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| Keywords: | glycerol borate glycerol ester of boric acid oil surfactant catalysis synthesis esterification |
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