| 多孔型阳极氧化铝膜的制备及微观分析 |
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| 引用本文： | 施云波,吕芳,冯侨华,王立权.多孔型阳极氧化铝膜的制备及微观分析[J].长春理工大学学报,2010,33(1):85-88. |
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| 作者姓名： | 施云波 吕芳 冯侨华 王立权 |
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| 作者单位： | 哈尔滨工程大学机械工程博士后科研流动站,哈尔滨,150001;哈尔滨理工大学测控技术与通信工程学院,哈尔滨,150080;哈尔滨理工大学应用科学学院,哈尔滨,150080;哈尔滨理工大学测控技术与通信工程学院,哈尔滨,150080;哈尔滨工程大学机械工程博士后科研流动站,哈尔滨,150001 |
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| 基金项目： | 国家自然科学基金资助项目(60772019);;中国博士后科学基金面上资助项目(20080440839);;黑龙江省博士后资助项目(LBH-Z08231);;黑龙江省教育厅科学技术研究项目(11541047) |
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| 摘 要： | 在硫酸电解液、草酸和磷酸电解液中,采用阳极氧化方法制备多孔型氧化铝膜。通过扫描电子显微镜对多孔型氧化铝膜进行形貌表征。根据试验得到:当0.3mol/L硫酸中,恒压25V阳极氧化1h可得到孔径约为40～60nm多孔氧化铝膜。在电解液为10.0g/L草酸与3.0ml/L磷酸混合液中,恒压140V二次阳极氧化可得到孔径为160～190nm多孔氧化铝膜。讨论了高温退火及磷酸处理对多孔氧化铝膜的影响,并进行了机理分析。
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| 关 键 词： | 铝 阳极氧化 多孔型氧化铝 |
The Fabrication of Porous Anodic Alumina Film and Micro-Analysis |
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| SHI Yunbo,LV Fang,FENG Qiaohua,WANG Liquan.The Fabrication of Porous Anodic Alumina Film and Micro-Analysis[J].Journal of Changchun University of Science and Technology,2010,33(1):85-88. |
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| Authors: | SHI Yunbo LV Fang FENG Qiaohua WANG Liquan |
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| Affiliation: | 1.Mechanical engineering postdoctoral research flow station;Harbin Engineering University;Harbin 150001;2.Applied Science College;Harbin Univ. Sci. Tech.;Harbin 150080;3. Measurement-Control Tech & Communications Engineering College;The higher educational key laboratory for Measuring & Control Technology and Instrumentations of Heilongjiang Province;Harbin Univ. Sci. Tech. Harbin 150080 |
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| Abstract: | The sulfuric acid and the mixture acid of oxalate and phosphate acid were used as electrolyte in the experiments, and the oxidation method was adopted to fabricate porous anodic alumina film. Scanning electron microscopy(SEM) was used to characterize porous anodic alumina film. According to the experiments,when the condition is that the voltage is 25V,the sulfuric acid concentration is 0.3mol/L,and the time is 1hour,the diameter of nanopores was about 40-60nm. When the condition is that the voltage is 140V,... |
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| Keywords: | Aluminum anodic oxidation porous anodic alumina film |
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