| LC/MS/MS法测定白酒中氨基甲酸酯类农残研究 |
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| 引用本文： | 何开蓉,程铁辕,张莹,夏于林.LC/MS/MS法测定白酒中氨基甲酸酯类农残研究[J].食品研究与开发,2019,40(15):156-159. |
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| 作者姓名： | 何开蓉 程铁辕 张莹 夏于林 |
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| 作者单位： | 食品安全检测四川省重点实验室;国家酒类检测重点实验室 |
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| 摘 要： | 首次建立同时对蒸馏白酒中8种氨基甲酸酯类农药(抗蚜威、恶虫威、克百威、仲丁威、甲萘威、扑灭威、多菌灵、灭多威)残留的液相色谱串联质谱法(liquid chromatography-tandem mass spectrometry, LC/MS/MS)定性鉴别和定量测试方法,此8种农药残留的方法检出限为0.5 μg/kg^10 μg/kg。上述8种农药残留在蒸馏白酒中加标回收率为87.6 %~100.0 %,精密度为0.89 %~5.6 %,均能够满足测试要求。
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| 关 键 词： | 液相色谱串联质谱联用仪 白酒 农药残留 定量分析 |
| 收稿时间： | 2018/10/11 0:00:00 |
Research of Analysis of Carbamic Ester Pesticide Residues in Liquor by LC/MS/MS |
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| HE Kai-rong,CHENG Tie-yuan,ZHANG Ying,XIA Yu-lin.Research of Analysis of Carbamic Ester Pesticide Residues in Liquor by LC/MS/MS[J].Food Research and Developent,2019,40(15):156-159. |
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| Authors: | HE Kai-rong CHENG Tie-yuan ZHANG Ying XIA Yu-lin |
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| Affiliation: | (Food Safety Detection Key Laboratory of Sichuan Province, Chengdu 610000, Sichuan, China;The State Key Lab of Liquor Products Test, Yibin 644000,S ichuan, China) |
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| Abstract: | HE Kai-rong;CHENG Tie-yuan;ZHANG Ying;XIA Yu-lin(Food Safety Detection Key Laboratory of Sichuan Province, Chengdu 610000, Sichuan, China;The State Key Lab of Liquor Products Test, Yibin 644000,S ichuan, China) |
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| Keywords: | liquid chromatography-tandem mass spectrometry(LC/MS/MS) liquor pesticide residues quantitative analysis |
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