Synthesis and structural characterization of Na2MnP2O7 crystal |
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| Authors: | N. K. Lokanath M. A. Sridhar J. ShashidharA Prasad G. S. Gopalakrishna K. G. Ashamanjari |
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| Affiliation: | (1) Department of Studies in Physics, University of Mysore, Manasagangotri, 570 006 Mysore, India;(2) Department of Studies in Geology, University of Mysore, Manasagangotri, 570 006 Mysore, India |
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| Abstract: | Na2MnP2O7 crystals were synthesized by hydrothermal technique. Crystals obtained are in the form of single crystals of rhombohedral morphology with lattice parameters as follows: triclinic, P 1, π = 0-71069 Å, a = 6.657(3) Å, b = 6.714(6) Å, c = 6.518(4) Å, α = 112.31(6)°, β = 92.14(4)°, γ = 83.89(5)°, V = 268.0(3) Å3, Z = 2, ρcal = 2, 3.121 g/cm3, μ = 3.121 mm-1, F000 = 244, goodness-of-fit on F = 1.348, final R indices with [I > 3σ(I)]R = 0051 and ωR = 0.065. |
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| Keywords: | NASICON hydrothermal crystal structure |
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