| 微波辐射下固相合成乙酰基二茂铁-DL-甘氨酸缩合物 |
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| 引用本文： | 吴校彬,袁海龙.微波辐射下固相合成乙酰基二茂铁-DL-甘氨酸缩合物[J].化学与生物工程,2009,26(3). |
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| 作者姓名： | 吴校彬 袁海龙 |
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| 作者单位： | 黄冈师范学院化学与应用化学学院,湖北,黄州,438000 |
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| 基金项目： | 湖北省教育厅科学研究项目 |
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| 摘 要： | 在氧化铝存在下,以乙酰基二茂铁、DL-甘氨酸为原料,在微波辐射条件下采用固相合成方法制备了乙酰基二茂铁-DL-甘氨酸缩合物.通过元素分析、红外光谱和核磁共振谱对产物的结构进行了表征;对合成条件进行了初步探讨.
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| 关 键 词： | 固相合成 微波 二茂铁 甘氨酸 |
Solid Phase Synthesis of Acetyl Ferrocene-Glycine Condensate under Microwave Irradiation |
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| WU Xiao-bin,YUAN Hai-long.Solid Phase Synthesis of Acetyl Ferrocene-Glycine Condensate under Microwave Irradiation[J].Chemistry & Bioengineering,2009,26(3). |
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| Authors: | WU Xiao-bin YUAN Hai-long |
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| Affiliation: | College of Chemistry and Applied Chemistry;Huanggang Normal University;Huangzhou 438000;China |
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| Abstract: | Acetyl ferrocence-glycine condensate was prepared by solid phase synthesis method using acetyl ferrocence and glycine as raw materials by microwave irradiation with the exsisting of Al2O3.The structure of acetyl ferrocence-glycine condensate was characterized by elementary analysis,IR and 1HNMR.The preparation conditions of the condensate were discussed briefly. |
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| Keywords: | solid phase synthesis microwave ferrocence glycine |
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