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凝固速率对Si-Ta合金固液界面稳定性的影响
引用本文:崔春娟,张军,吴昆,邹德宁,刘林,傅恒志.凝固速率对Si-Ta合金固液界面稳定性的影响[J].材料工程,2012(8):60-64.
作者姓名:崔春娟  张军  吴昆  邹德宁  刘林  傅恒志
作者单位:1. 西安建筑科技大学冶金工程学院,西安710055;西北工业大学凝固技术国家重点实验室,西安710072
2. 西北工业大学凝固技术国家重点实验室,西安,710072
3. 西安建筑科技大学冶金工程学院,西安,710055
基金项目:国家自然科学基金资助项目,高等学校博士学科点专项科研基金新教师基金资助,陕西省自然科学专项研究基金资助,陕西省教育厅专项科研基金,西安建筑科技大学科技计划资助项目(人才科技基金RC0907)
摘    要:以Si-Ta合金为研究对象,采用零功率法研究凝固速率对定向凝固固液界面稳定性的影响。结果表明:当凝固速率在0.3~9.0mm/min范围内,随着凝固速率的增大,固液界面经历了平界面→浅胞状界面→锯齿状界面→浅胞状界面→平界面的演化规律。在较低的凝固速率范围之内,实验结果与理论计算基本吻合。然而,在较高凝固速率时,实验结果与理论计算出现偏差,这是由于热力学和动力学均发生变化,使得在凝固速率V=5.0mm/min时固液界面就已经达到了稳定的平界面。

关 键 词:定向凝固  电子束悬浮区熔  凝固速率  固液界面

Influence of Solidification Rate on Solid-liquid Interface of Si-Ta Alloy
CUI Chun-juan , ZHANG Jun , WU Kun , ZOU De-ning , LIU Lin , FU Heng-zhi.Influence of Solidification Rate on Solid-liquid Interface of Si-Ta Alloy[J].Journal of Materials Engineering,2012(8):60-64.
Authors:CUI Chun-juan  ZHANG Jun  WU Kun  ZOU De-ning  LIU Lin  FU Heng-zhi
Affiliation:1 School of Metallurgical Engineering,Xi’an University of Architecture and Technology,Xi’an 710055,China;2 State Key Laboratory of Solidification Processing,Northwestern Polytechnical University,Xi’an 710072,China)
Abstract:The influence of solidification rate on the solid-liquid interface of Si-Ta alloy was studied by the zero power method.The results show that the solid-liquid interface morphology has the following evolution processing: planar interface→shallow cell interface→cell interface→shallow cell interface→planar interface when the solidification rate varies from 0.3mm/min to 9.0mm/min.At the lower solidification rates,the experiment results can be consistent with Jackson-Hunt theory well.However,there is a deviation between the theory calculation and the experiment at the higher solidification rates.This is caused by the change of the thermodynamics and kinetics,and the solid-liquid interface can get to planar interface at the solidification rate V=5.0mm/min.
Keywords:directional solidification  electron beam floating zone melting  solidification rate  solid-liquid interface
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