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超声波改性珠蚌多肽与钙离子的螯合
引用本文:王辉,涂宗财,叶云花,刘光宪,李春平,胡月明.超声波改性珠蚌多肽与钙离子的螯合[J].食品与发酵工业,2013,39(4):12-16.
作者姓名:王辉  涂宗财  叶云花  刘光宪  李春平  胡月明
作者单位:1. 南昌大学生物质转化教育部工程研究中心,食品科学与技术国家重点实验室,江西南昌,330047
2. 南昌大学生物质转化教育部工程研究中心,食品科学与技术国家重点实验室,江西南昌,330047;江西师范大学,江西南昌,330022
3. 江西师范大学,江西南昌,330022
4. 江西省农业科学院农产品加工中心,江西南昌,330000
基金项目:国家"863"项目"新型水产品加工装备开发与新技术研究",江西省教育厅项目"珍珠加工废弃物的高值化综合利用技术研究"
摘    要:以珠蚌多肽为原料,研究超声波改性珠蚌多肽与钙的螯合能力,并对改性多肽与肽钙螯合物的结构进行初探。研究表明:超声波改性珠蚌多肽的最佳工艺为,超声功率160 W、超声时间10 min、超声温度50℃、液固比40∶1(mL∶g),此时钙质量分数达到6.037%。通过FTIR、UV、SEM等技术对改性多肽及其肽钙进行分析,FT-IR分析得出羧基参与肽钙螯合反应生成羧酸盐;UV分析得出改性多肽与钙离子通过配位键结合形成肽钙螯合物;SEM分析表明改性肽钙的结构类似于盐类。

关 键 词:超声波  改性  肽钙  珠蚌多肽

Study on oyster peptide chelating calcium by ultrasonic
Wang Hui,Tu Zong-cai,Ye Yun-hua,Liu Guang-xian,Li Chun-ping,Hu Yue-ming.Study on oyster peptide chelating calcium by ultrasonic[J].Food and Fermentation Industries,2013,39(4):12-16.
Authors:Wang Hui  Tu Zong-cai  Ye Yun-hua  Liu Guang-xian  Li Chun-ping  Hu Yue-ming
Affiliation:1(Engineering Research Center for Biomass Conversion,State Key Laboratory of Food Science and Technology,Nanchang University,Nanchang 330047,China) 2(Jiangxi Normal University,Nanchang 330022,China) 3(Food Research Centre,Jiangxi Academy of Agricultural Sciences,Nanchang 330200,China)
Abstract:The influence of ultrasonic pretreatment on modified oyster peptide binding calcium capacity during oyster peptide process was studied.The structural characterization of the modified peptide chelating calcium was also studied using the spectra technologies.The results showed that the optimum processing of modified peptide were as follows: 80% of ultrasonic power,ultrasonic time of 10min,ultrasonic temperature 50 ℃,liquid-solid ratio 40:1.Under the above conditions,the quality score of calcium is 6.037%.FT-IR,UV and environmental scanning electron microscope(SEM) were used to study the characterization of the modified peptide and modified peptide calcium.FI-IR spectrum indicated that the carboxyl group can participate in the reaction to form carboxylate.UV spectrum indicated that the peptide and calcium chelate was formed by modified peptide and calcium through coordination bonds.SEM showed that microstructure of modified peptide and calcium chelate was similar to that of salt.
Keywords:ultrasonic  modified  peptide-calcium  oyster peptide
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