| 2,3-戊二酮的合成 |
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| 引用本文： | 赵延伟,贾卫民,王之建,梁立冬.2,3-戊二酮的合成[J].化学试剂,2012,34(5):479-480. |
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| 作者姓名： | 赵延伟 贾卫民 王之建 梁立冬 |
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| 作者单位： | 上海应用技术学院上海香料研究所,上海,200235 |
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| 摘 要： | 以丙酸甲酯为原料经Claisen缩合、肟化和肟交换反应合成了标题化合物。其结构经MS、1HNMR和13CNMR确定。
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| 关 键 词： | 2 3-戊二酮 2-甲基-3-氧代戊酸甲酯 丙酸甲酯 合成 |
Synthesis of 2, 3-pentanedione |
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| ZHAO Yan-wei
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JIA Wei-min
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WANG Zhi-jian
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LIANG Li-dong.Synthesis of 2, 3-pentanedione[J].Chemical Reagents,2012,34(5):479-480. |
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| Authors: | ZHAO Yan-wei JIA Wei-min WANG Zhi-jian LIANG Li-dong |
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| Affiliation: | (Shanghai Research Institute of Fragrance & Flavor Industry,Shanghai Institute of Technology School,Shanghai 200235,China) |
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| Abstract: | 2,3-Pentanedione was synthesized from methyl proionate by Claisen condensation reaction,oximation and oxime exchange reaction.The compound was characterized by MS,1HNMR,and 13CNMR. |
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| Keywords: | 2 3-pentanedione 2-methyl-3-oxomethylvalerate methyl proionate synthesis |
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