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Low‐temperature molten salt synthesis of forsterite powders with controllable morphology
Authors:Zhou Fu Wang  Mei Jing Chen  Yan Ma  Hao Liu  Chun Hui Han  Xi Tang Wang
Affiliation:The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan, People's Republic of China
Abstract:Forsterite powders with controllable morphology were synthesized using oxides as raw materials in NaCl–KCl molten salt media. The effects of MgO/SiO2 ratio, calcining temperature, and salt/oxide ratio on the phase composition and morphology of the powders are investigated. The results indicate that single‐phase forsterite powders can be synthesized from a mixture of MgO and SiO2 with a MgO/SiO2 molar ratio of 2:1.3 at 700°C. With the increase in calcining temperature, the powders obtained changes from an irregular to a columnar morphology. In addition, the morphology of the forsterite powders produced can also be controlled by altering the salt/oxide ratio.
Keywords:powders  silicates  morphology  synthesis
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