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Surface Oxidation of Al2O3/SiC Nanocomposite: Phase Transformation and Microstructure
引用本文:蔡舒 彭珍珍 冯杰 鲁枫. Surface Oxidation of Al2O3/SiC Nanocomposite: Phase Transformation and Microstructure[J]. 中国稀土学报(英文版), 2005, 23(4): 429-432
作者姓名:蔡舒 彭珍珍 冯杰 鲁枫
作者单位:School of Material Science and Engineering,Tianjin University,Tianjin 300072,China,School of Material Science and Engineering,Tianjin University,Tianjin 300072,China,School of Material Science and Engineering,Tianjin University,Tianjin 300072,China,School of Material Science and Engineering,Tianjin University,Tianjin 300072,China
基金项目:国家高技术研究发展计划(863计划)
摘    要:The surface oxidation behavior of pressureless sintered Al2O3/SiC nanocomposite was studied from 1000 to 1400 ℃ for more than 10 h in air. Weight gain during the process of heat treatment was measured by TG analysis. Phase transformation and microstructure changes of these specimens due to oxidation were investigated with X-ray diffraction (XRD), SEM and EDX technology. Thermogravimetric analysis show that the weight gain as a result of oxidation of SiC become significant above 1200 ℃. In the range of 1000~1300 ℃, the SiC grits are usually coated with a layer of amorphous silica after oxidation. Above 1300 ℃, the amorphous silica reacted with alumina matrix and formed mullite or crystallized into cristobalite. The rate of oxidation depends on the formation of dense cristobalite film. Large amount of needle-like mullite and alumina crystals are formed on the surface after oxidation at 1400 ℃.

关 键 词:Al2O3/SiC 纳米复合材料 表面氧化 热处理 稀土 显微结构 相变
文章编号:1002-0721(2005)04-0429-04
收稿时间:2004-11-10
修稿时间:2005-04-30

Surface Oxidation of Al2O3/SiC Nanocomposite: Phase Transformation and Microstructure
CAI Shu,PENG Zhenzhen,Feng Jie,Lu Feng. Surface Oxidation of Al2O3/SiC Nanocomposite: Phase Transformation and Microstructure[J]. Journal of Rare Earths, 2005, 23(4): 429-432
Authors:CAI Shu  PENG Zhenzhen  Feng Jie  Lu Feng
Abstract:
Keywords:nanocomposites  surface  oxidation  heat treatment  rare earths
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