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金属玻璃基复合材料的制备及断裂韧性测试
引用本文:李春燕,寇生中,赵燕春,刘广桥,丁雨田. 金属玻璃基复合材料的制备及断裂韧性测试[J]. 功能材料, 2012, 43(10): 1344-1347. DOI: 10.3969/j.issn.1001-9731.2012.10.030
作者姓名:李春燕  寇生中  赵燕春  刘广桥  丁雨田
作者单位:1.兰州理工大学甘肃省有色金属新材料省部共建国家重点实验室,甘肃兰州730050 兰州理工大学有色金属合金及加工教育部重点实验室,甘肃兰州730050;2.兰州理工大学甘肃省有色金属新材料省部共建国家重点实验室,甘肃兰州730050 兰州理工大学有色金属合金及加工教育部重点实验室,甘肃兰州730050;3.兰州理工大学甘肃省有色金属新材料省部共建国家重点实验室,甘肃兰州730050 兰州理工大学有色金属合金及加工教育部重点实验室,甘肃兰州730050;4.兰州理工大学甘肃省有色金属新材料省部共建国家重点实验室,甘肃兰州730050 兰州理工大学有色金属合金及加工教育部重点实验室,甘肃兰州730050;5.兰州理工大学甘肃省有色金属新材料省部共建国家重点实验室,甘肃兰州730050 兰州理工大学有色金属合金及加工教育部重点实验室,甘肃兰州730050
基金项目:国家自然科学基金资助项目(50961008,51061008);国家重点基础研究发展计划(973计划)前期研究专项资助项目(2011CB612203)
摘    要:采用铜模吸铸法制备了(Zr0.55Al0.1Ni0.05Cu0.30)100-xTix(x=0、2、4、6、8)板状哑铃型金属玻璃基复合材料试样。用X射线衍射(XRD)、岛津AG-10TA万能材料力学试验机和JSM-6700F场发射扫描电子显微镜(SEM)对试样的组织结构以及断裂韧性进行了测试。结果表明,当x=0、2、4时,试样为非晶-晶体复合材料,当x=6、8时,试样为晶体材料。表明通过调整Ti的含量可以制备出金属玻璃基复合材料。采用三点弯曲法测定了复合材料的断裂韧性,当x=0、2、4时,试样的断裂韧性KIC值分别为10.529、5.142和3.446MPa.m1/2。

关 键 词:金属玻璃  复合材料  制备  微观组织  断裂韧性

Preparation of metallic glass based composites and measurement of the fracture toughness
LI Chun-yan,KOU Sheng-zhong,ZHAO Yan-chun,LIU Guang-qiao,DING Yu-tian. Preparation of metallic glass based composites and measurement of the fracture toughness[J]. Journal of Functional Materials, 2012, 43(10): 1344-1347. DOI: 10.3969/j.issn.1001-9731.2012.10.030
Authors:LI Chun-yan  KOU Sheng-zhong  ZHAO Yan-chun  LIU Guang-qiao  DING Yu-tian
Affiliation:1,2(1.State Key Laboratory of Gansu Advanced Non-ferrous Metal Materials, Lanzhou University of Technology,Lanzhou 730050,China; 2.Key Laboratory of Non-ferrous Metal Alloys and Processing of the Ministry of Education, Lanzhou University of Technology,Lanzhou 730050,China)
Abstract:The dumbbell-shaped metallic glass based composites of(Zr0.55Al0.1Ni0.05Cu0.30)100-xTix(x=0,2,4,6,8) were prepared by copper mold casting method.Microstructure and fracture toughness of samples were studied by X-ray diffraction(XRD),universal testing machine and scanning electron microscope(SEM).The results indicate that metallic glass based composites can be fabricated by adjusting Ti addition.The structure of the alloys were composed of metallic glass and crystal when the Ti content was x=0,2,4 and the structure of the alloys were crystal when the Ti content was x=6,8.The fracture toughness of composites which Ti content was x=0,2,4 were measured by three point bending method,and the KIC value were 10.529,5.142 and 3.446 MPa·m1/2 respectively.
Keywords:metallic glass  composites  preparation  microstructure  fracture toughness
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