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火焰原子吸收光谱法测定铜锍中银
引用本文:李静.火焰原子吸收光谱法测定铜锍中银[J].黄金,2017,38(3).
作者姓名:李静
作者单位:中条山有色金属集团有限公司
摘    要:建立了火焰原子吸收光谱法测定铜锍中银的分析方法,样品经硝酸、高氯酸溶解,在15%盐酸介质中,采用原子吸收光谱法测定银。标准曲线相关系数为0.999 9,线性范围为20.0~300.0 g/t,相对标准偏差(RSD)2.02%~3.07%,加入标准物质回收率为99.3%~103.1%。该方法简单快速、准确可靠,适用于铜锍中银量的测定。

关 键 词:火焰原子吸收光谱法  铜锍    测定介质  干扰因素

Determination of silver in copper matte by flame atomic absorption spectrometry
Li Jing.Determination of silver in copper matte by flame atomic absorption spectrometry[J].Gold,2017,38(3).
Authors:Li Jing
Abstract:Flame atomic absorption spectrometry is established to determine silver in copper matte.The samples are dissolved by nitric acid and perchloric acid,and in 15 % hydrochloric acid medium,silver is determined by atomic absorption spectrometry.The correlation coefficient of the standard curve is 0.999 9,the linear range is 20.0-300.0 g/t,the relative standard deviation is 2.02% - 3.07 % . and the recovery rate of standard substance is 99.3%- 103.1%.The method is simple ,fast , accurate and reliable,and is suitable for the determination of silver in copper matte.
Keywords:flame atomic absorption spectrometry  copper matte  silver  determination medium  interferehce factor
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