吸附分离法脱除环氧丙烷中微量水的研究 |
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引用本文: | 张俊宏,刘靖,王祥生,张永春,郭新闻.吸附分离法脱除环氧丙烷中微量水的研究[J].应用化工,2003,32(4):20-22. |
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作者姓名: | 张俊宏 刘靖 王祥生 张永春 郭新闻 |
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作者单位: | 1. 大连理工大学,精细化工国家重点实验室,辽宁,大连,116012 2. 大连理工绿源环保产业有限公司,辽宁,大连,116012 |
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基金项目: | 国家重点基础研究发展规划资助项目(G2000048009) |
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摘 要: | 研究了用预处理后的5A分子筛、002×7K吸附树脂脱除环氧丙烷中微量水。结果表明,在合适的操作温度、进料线速率等条件下,5A分子筛和002×7K吸附树脂都能使环氧丙烷中水含量降到符合GB/T14491 2001要求的工业用优级环氧丙烷标准,002×7K吸附树脂在一定条件下性能更为优异。实验还考虑了吸附剂循环利用情况,结果表明,前70次再生后的吸附剂吸附分离效率略有下降。
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关 键 词: | 5A分子筛 吸附树脂 环氧丙烷 微量水 分离 |
文章编号: | 1671-3206(2003)04-0020-03 |
修稿时间: | 2003年3月4日 |
Study on removal of trace water in propylene oxide with adsorption stripping |
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Abstract: | The removal of trace water in propylene oxide with prepared 5A molecular sieve and 002×7K adsorbent resin is studied.The resuts showed that both the two adsorbents have the capability of removing trace water in propylene oxide to a relatively low level when the operation temperature and linear velocity are of particular significance,which meets the standard of GB/T 14491 2001 for the superior quality product.Moreover,the 002×7K adsorbent resin performs is better.The regeneration and recycle of adsorbents are tested,the results showed that the efficiency of the reused adsorbents was droped slightly after 70 times regeneration. |
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Keywords: | 5A molecular sieve adsorbent resin propylene oxide trace water separation |
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