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Determination of Trace Rare Earth Elements in Biological Samples by ICP-AES with Tungsten-spiral Electrothermal Vaporization Sampling
引用本文:梅二文,刘慧,廖振环,江祖成. Determination of Trace Rare Earth Elements in Biological Samples by ICP-AES with Tungsten-spiral Electrothermal Vaporization Sampling[J]. 中国稀土学报(英文版), 1993, 0(1)
作者姓名:梅二文  刘慧  廖振环  江祖成
作者单位:Department of chemistry wuhan University,Wuhan 430072,China,Department of chemistry,wuhan University,Wuhan 430072,China,Department of chemistry,wuhan University,Wuhan 430072,China,Author to whom correspondence should be sent
摘    要:A method for determination of trace rare earth elements in biological sample by ICP-AES withtungsten-spiral electrothermal vaporization(TETV-ICP-AES)sampling has been developed in this work.Several influencing factors including desolvation and vaporization parameters,carrier gas flow rate and ma-trix effect were investigated in detail.Under optimal experimental conditions,the detection limits for La,Nd,Gd,Dy,Ho,Yb,Lu and Y were obtained in the range of 10~(-9)~10~(-11) g,and they are comparable to and,inmost instances,better than those for the GFAAS and conventional pneumatic nebulisation-ICP-AES.Theprecision(RSD)obtained for this method is less than 6%.


Determination of Trace Rare Earth Elements in Biological Samples by ICP-AES with Tungsten-spiral Electrothermal Vaporization Sampling
Mei Er-Wen Liu Hui Liao Zhen-Huan Jiang Zu-Cheng. Determination of Trace Rare Earth Elements in Biological Samples by ICP-AES with Tungsten-spiral Electrothermal Vaporization Sampling[J]. Journal of Rare Earths, 1993, 0(1)
Authors:Mei Er-Wen Liu Hui Liao Zhen-Huan Jiang Zu-Cheng
Affiliation:Mei Er-Wen Liu Hui Liao Zhen-Huan Jiang Zu-Cheng Department of Chemistry,Wuhan University,Wuhan 430072,China Author to whom correspondence should be sent
Abstract:
Keywords:Tungsten-spiral electrothermal vaporization sampling  ICP-AES  REE  Biological sample
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