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IAEA国际比对样品的γ谱分析
引用本文:吴云锋,杜金洲,黄德坤,张经.IAEA国际比对样品的γ谱分析[J].核化学与放射化学,2009,31(3):157-162.
作者姓名:吴云锋  杜金洲  黄德坤  张经
作者单位:华东师范大学 河口海岸学国家重点实验室,上海 200062
基金项目:中国重点基础发展计划资助项目,上海市浦江人才计划资助项目,教育部留学回国人员基金 
摘    要:本实验室使用超低本底HPGe γ谱仪参加了2006年IAEA组织的γ核素放射性活度测量比对.按比对要求测量了土壤和水样中54Mn, 60Co, 65Zn, 134Cs, 137Cs, 241Am, 109Cd, 210Pb以及草样中的40K, 137Cs.使用无源效率刻度软件LabSOCS对HPGe γ谱仪进行效率刻度,γ谱分析采用Genie 2000分析软件.与IAEA的参考值相比,本实验室报出的测量值的总体接受率为89%,不被接受率为0,高于327个参加比对实验室分析结果为64%的总体可接受率,明显低于29%的总体不被接受率.

关 键 词:环境样品  国际比对  γ核素  无源效率刻度  

Gamma Spectrum Analysis of IAEA International Intercomparison Samples
WU Yun-feng,DU Jin-zhou,HUANG De-kun,ZHANG Jing.Gamma Spectrum Analysis of IAEA International Intercomparison Samples[J].Journal of Nuclear and Radiochemistry,2009,31(3):157-162.
Authors:WU Yun-feng  DU Jin-zhou  HUANG De-kun  ZHANG Jing
Affiliation:State Key Laboratory of Estuarine and Coastal Research, East China Normal University, Shanghai 200062, China
Abstract:In 2006, the international intercomparision of gamma-radionuclides was conducted by ultra-low background HPGe γ- spectrometer systems in our lab. According to IAEA’s rules, activities of 54Mn, 60Co, 65Zn, 134Cs, 137Cs, 241Am, 109Cd, and 210Pb in soil and water, and 40K, 137Cs in grass have to be measured. The activies of these radionuclides were performed by Genie 2000 for γ-spectra analysis and by LabSOCS for efficiency calibration. Our laboratory obtained excellent scores with 89% for acceptable and 0 for not acceptable. The percentage of acceptable is obviously higher than average value 64% in all the participant labs, while those of not acceptable are lower than average 29%.
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