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PNN-PZT陶瓷流延浆料流变性能研究
引用本文:李勇君,裘进浩,朱孔军,季宏丽.PNN-PZT陶瓷流延浆料流变性能研究[J].电子元件与材料,2008,27(12).
作者姓名:李勇君  裘进浩  朱孔军  季宏丽
作者单位:南京航空航天大学,智能材料与结构航空科技重点实验室,江苏,南京,210016
基金项目:江苏省自然科学基金,航空基础科学基金
摘    要:以体积比为7:3的丁酮和无水乙醇为混合溶剂,聚乙烯醇缩丁醛(PVB)为粘结剂,邻苯二甲酸二丁酯为增塑剂,玉米油为分散剂配制了PNN-PZT陶瓷流延浆料。研究了浆料球磨时间、固相体积分数以及各有机添加剂用量对其流变性能的影响。结果表明:当w(分散剂)为0.75%,w(粘结剂)为4.17%,球磨时间为8h,固相体积分数为75%,ζ(增塑剂:粘结剂)为0.6时,浆料流变性能良好,浆料黏度在2500mPa·s左右。

关 键 词:PNN-PZT  流延成型  流变性能  黏度

Study on rheological behaviors of slurry for tape casting PNN-PZT ceramics
LI Yong-jun,QIU Jin-hao,ZHU Kong-jun,JI Hong-li.Study on rheological behaviors of slurry for tape casting PNN-PZT ceramics[J].Electronic Components & Materials,2008,27(12).
Authors:LI Yong-jun  QIU Jin-hao  ZHU Kong-jun  JI Hong-li
Affiliation:LI Yong-jun,QIU Jin-hao,ZHU Kong-jun,JI Hong-li (The Aeronautical Key Laboratory for Smart Materials , Structures,Nanjing University of Aeronautics , Astronautics,Nanjing 210016,China)
Abstract:Slurry for tape casting PNN-PZT ceramics was prepared using the butanone and anhydrous ethanol (volume ratio of 7:3) as mixed solvent,and poly vinyl butyral (PVB),dibutyl phthalate and corn oil were used as a binder,a plasticizer and a dispersant respectively. The effects of ball milling time,solid phase volume fraction and each organic additives amouts on the rheological behaviors of slurry were studied. The results show that the rheological behaviors are well with slurry viscosity of about 2 500 mPa·s when w (dispersant) is 0.75%,w (binder) is 4.17%,the ball milling time is 8 h,the solid phase volume fraction is 75%,and the ζ (plasticizer : binder) is 0.6.
Keywords:PNN-PZT
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