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摇铃状Fe_3O_4@C复合材料的结构表征及其储锂性能研究
引用本文:刘美梅,陈国新.摇铃状Fe_3O_4@C复合材料的结构表征及其储锂性能研究[J].电子显微学报,2014(3):209-214.
作者姓名:刘美梅  陈国新
作者单位:[1]中国科学院福建物质结构研究所,福建福州350002 [2]中国科学院宁波材料技术与工程研究所,浙江宁波315201
基金项目:国家自然科学基金资助项目(No.21271170).
摘    要:本文采用简易湿化学法制备新颖的摇铃状Fe3O4@C纳米复合材料。利用X射线衍射仪(XRD)和透射电子显微镜(TEM)技术对其形貌、成分及微观结构进行表征,并对复合材料进行电池性能测试。结果表明,由于Fe3O4@C纳米复合材料独特的摇铃状结构,其作为锂离子电池负极表现出良好的电化学性能,具有良好的循环稳定性和较高的比容量。

关 键 词:摇铃状FeO@C  TEM  XRD  循环稳定性  比容量

Characterization and lithium storage performance of yolk-shell Fe3 O4@C nanocomposite
LIU Mei-meiFujian Institute of Research on the Structure of Matter,Chinese Academy of Sciences,Fuzhou Fujian,CHEN Guo-xin.Characterization and lithium storage performance of yolk-shell Fe3 O4@C nanocomposite[J].Journal of Chinese Electron Microscopy Society,2014(3):209-214.
Authors:LIU Mei-meiFujian Institute of Research on the Structure of Matter  Chinese Academy of Sciences  Fuzhou Fujian  CHEN Guo-xin
Affiliation:(Ningbo Institute of Material Technology and Engineering, Chinese Academy of Sciences, Ningbo Zhejiang 315201 , China)
Abstract:In this paper,a novel yolk-shell Fe3O4@C composite had been synthesized via a simple wet chemical method.The morphologies,microstructures and chemical composition of Fe3 O4@C were characterized by transmission electron microscopy (TEM) and X-ray diffraction (XRD).The Fe3 O4@C composite exhibited an excellent electrochemical performance as anode of lithium-ion battery (LIBs) with an excellent cyclic stability and high capacity,due to the unique yolk-shell structure.
Keywords:yolk-shell Fe3O4@C  TEM  XRD  cyclic stability  capacity
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