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热酸浸出—铁矾法炼锌工艺中富集锗的研究
引用本文:何静,鲁君乐,刘中清,唐谟堂,杨声海,姚维义,陈慧光.热酸浸出—铁矾法炼锌工艺中富集锗的研究[J].广东有色金属学报,2002(Z1).
作者姓名:何静  鲁君乐  刘中清  唐谟堂  杨声海  姚维义  陈慧光
作者单位:中南大学冶金科学与工程系,中南大学冶金科学与工程系,四川会东铅锌矿,中南大学冶金科学与工程系,中南大学冶金科学与工程系,中南大学冶金科学与工程系,中南大学冶金科学与工程系 湖南长沙410083,湖南长沙410083,四川西昌615205,湖南长沙410083,湖南长沙410083,湖南
摘    要:进行了“热酸浸出—铁矾法炼锌工艺中锗和银的富集和回收”的实验室扩大试验 ,在 10个循环试验中 ,工艺流程畅通 ,以黄钾铁矾沉铁代替通常的钠或铵铁矾沉铁使锗在矾渣中的损失减少到 5 0 %以下 ,锗和银均富集于高酸浸出渣中 ,其品位分别为 0 0 32 5 %和 0 16 2 %.

关 键 词:酸浸  铁矾法  富集  

Study on enrichment of germaniumin hot acid leaching and zinc-smelting with iron vitriol method
HE Jing ,LU Jun-le ,LIU Zhong-qing ,TANG Mo-tang ,YANG Sheng-hai ,YAO Wei-yi ,CHEN Hui-guang.Study on enrichment of germaniumin hot acid leaching and zinc-smelting with iron vitriol method[J].Journal of Guangdong Non-Ferrous Metals,2002(Z1).
Authors:HE Jing  LU Jun-le  LIU Zhong-qing  TANG Mo-tang  YANG Sheng-hai  YAO Wei-yi  CHEN Hui-guang
Affiliation:HE Jing 1,LU Jun-le 1,LIU Zhong-qing 2,TANG Mo-tang 1,YANG Sheng-hai 1,YAO Wei-yi 1,CHEN Hui-guang 1
Abstract:The bench-scale experiment was conducted for enrichment and recovery of germanium in hot acid leaching and zinc-smelting with iron vitriol method. The flowsheet is smoothly during 10 periods of cyclic test. The loss of Ge in halotrichite residue was less than 5.0%, precipitating iron by using ferric potassium alum instead of common Na or ammonium alum. Ge and Ag were all enriched in the high acid leaching residue, and their grades are 0.0325% and 0.162%, respectively.
Keywords:acid leaching  iron vitriol method  up grade  germanium
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