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微量B对铸态TiAl基合金显微组织及热变形行为的影响
引用本文:李建波,刘咏,王岩,刘彬,杨广宇.微量B对铸态TiAl基合金显微组织及热变形行为的影响[J].粉末冶金材料科学与工程,2012(4):414-422.
作者姓名:李建波  刘咏  王岩  刘彬  杨广宇
作者单位:中南大学粉末冶金国家重点实验室;中南大学航空航天学院;日本东北大学金属研究院
基金项目:国家重点基础研究发展规划(973计划)资助项目(2011CB605505);国家高技术研究发展计划(863计划)资助项目(2008AA03A233);国家自然科学基金资助项目(51174233)
摘    要:采用电弧熔炼法制备含微量B元素的Ti-43Al-4Nb-1.4W-xB(x=0.2,0.4,0.6,0.8。数据为原子分数,%)合金;利用光学显微镜(OM)和扫描电镜(SEM)研究B含量对该铸态合金显微组织的影响,并通过热模拟压缩试验研究温度为1 050~1 200℃、应变速率为10 3~1 s 1的变形条件下Ti-43Al-4Nb-1.4W-0.6B合金的热变形行为,分析该合金在不同变形条件下的组织演化规律。结果表明:当B含量(质量分数)达到0.6%时,合金组织明显细化;Ti-43Al-4Nb-1.4W-0.6B合金的高温压缩流变应力随变形速率增加以及变形温度降低而增加;其峰值应力与变形条件之间的函数关系可用双曲正弦函数来描述,并以此求得高温变形激活能为580.68 kJ/mol;加入0.6%B对合金动态再结晶形核起到一定的促进作用,热变形后,合金发生明显的动态再结晶。

关 键 词:微量B  TiAl基合金  显微组织  热变形  变形激活能  动态再结晶

Effect of trace boron element on microstructure and hot deformation behaviors of as-cast TiAl based alloy
LI Jian-bo,LIU Yong,WANG Yan,LIU Bin,YANG Guang-yu.Effect of trace boron element on microstructure and hot deformation behaviors of as-cast TiAl based alloy[J].materials science and engineering of powder metallurgy,2012(4):414-422.
Authors:LI Jian-bo  LIU Yong  WANG Yan  LIU Bin  YANG Guang-yu
Affiliation:1(1.State Key Laboratory of Powder Metallurgy,Central South University,Changsha 410083,China;2.School of Aeronautics and Astronautics,Central South University,Changsha 410083,China;3.Institute of metals research,Tohoku University,Sendai 980-8577,Japan)
Abstract:The effect of B content on the microstructure and hot deformation behavors of as-cast Ti-43Al-4Nb-1.4W-xB alloy was systematically investigated using optical microscopy and scanning electron microscopy.The hot deformation behaviors of the Ti-43Al-4Nb-1.4W-0.6B alloy at temperatures from 1 050 ℃ to 1 200 ℃ with strain rates from 10 3to 1 s 1 were studied by thermal simulation compression tests.The results indicate that a refined microstructure for as-cast Ti-43Al-4Nb-1.4W-xB alloy can be obtained when the content of B reaches to 0.6%.The flow stress of Ti-43Al-4Nb-1.4W-0.6B alloy increases with increasing strain rate and decreasing deformation temperature.The relationship between peak stress and deformation conditions for the alloy can be described by a hyperbolic-sine type equation,and the apparent activation energy calculated is 580.68 kJ/mol.Dynamic recrystallization occurs apparently during hot deformation of the alloy.The addition of 0.6% B can accelerate the nucleation of dynamic recrystallization of the alloy.
Keywords:trace B element  TiAl based alloy  microstructure  hot deformation  deformation activation energy  dynamic recrystallization
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