Synthesis and characterization of mesostructured ceria-zirconia solid solution |
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Authors: | LI Changlin GU Xin WANG Yanqin WANG Yaojun WANG Yangang LIU Xiaohui LU Guanzhong |
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Affiliation: | Laboratory for Advanced Materials, Research Institute of Industrial Catalysis, East China University of Science and Technology, Shanghai 200237, China |
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Abstract: | Mesostructured Ce0.6Zr0.4O2 solid solutions were synthesized by coprecipitation combined with evaporation-induced self-assembly process. The obtained materials were characterized by X-ray diffractometer (XRD), Raman, transmission electron microscopy (TEM), N2 sorption, and hydrogen temperature programmed reduction (H2-TPR). The results showed that the solid solutions consisted of uniform nanocrystals, which piled homogeneous mesopores of about 4 nm. Furthermore, different surfactants had little influence on the mesoporous structures. All these samples exhibited high thermal stability. |
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Keywords: | mesostructured ceria-zirconia solid solution nanocrystals rare earths |
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