| 氟吗啉缩合新工艺的研究 |
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| 引用本文： | 孙德群,田爱俊,杨越.氟吗啉缩合新工艺的研究[J].现代农药,2009,8(2). |
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| 作者姓名： | 孙德群 田爱俊 杨越 |
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| 作者单位： | 1. 山东大学威海分校海洋学院,山东,威海,264209
2. 威海秀水药物研发有限公司,山东,威海,264209 |
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| 摘 要： | 在甲苯溶剂中,回流状态下,以氨基钠为碱催化缩合生成氟吗啉,所得产品含量用高效液相色谱定量分析高于95%,收率达80%。该方法未见国内外文献报道,具有高效、低成本、对环境友好的优点。
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| 关 键 词： | 工艺 氟吗啉 氨基钠 |
Novel Process of Condensation for Preparation of Flumorph |
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| SUN De-qun,TIAN Ai-jun,YANG Yue.Novel Process of Condensation for Preparation of Flumorph[J].Modern Agrochemicals,2009,8(2). |
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| Authors: | SUN De-qun TIAN Ai-jun YANG Yue |
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| Affiliation: | 1.Marine College;Shandong University at Weihai;Shandong Weihai 264209;China;2.Weihai Xiushui Pharmaceutical R & D Company;China |
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| Abstract: | Flumorph was prepared in a novel process,in which the sodium amide was employed as base and the toluene was used as solvent.The content and yield of the flumorph were reached over 95% and 80% respectively.This process has the advantage of low cast,effective produce and environment friendly while comparing with other related methods. |
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| Keywords: | process flumorph sodium amide |
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