| 15种邻苯二甲酸酯在液相色谱/串联质谱上的分离和系统干扰研究 |
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| 引用本文： | 夏春岚,任举,朱小梅,程天蓉.15种邻苯二甲酸酯在液相色谱/串联质谱上的分离和系统干扰研究[J].香料香精化妆品,2013(5):36-42. |
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| 作者姓名： | 夏春岚 任举 朱小梅 程天蓉 |
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| 作者单位： | 华宝食用香精香料有限公司,上海201821 |
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| 摘 要： | 用超高效液相色谱/三重四极杆质谱(UPLC-MS/MS)联用技术检测邻苯二甲酸酯类物质(PAEs)。考察流动相、柱子填料等因素对各化合物分离的影响,探讨了系统干扰的影响和解决方法,为建立液-质-质联用技术定量检测邻苯二甲酸酯类(PAEs)打下了基础。
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| 关 键 词： | 液相色谱/串联质谱联用 邻苯二甲酸酯(PAEs) 定量测定 |
Study on Separation of Fifteen Phthalates and System Interference by Using Liquid Chromatography/Tandem Mass Sectrometry |
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| XIA Chunlan,REN Ju,ZHU Xiaomei,CHENG Tianrong.Study on Separation of Fifteen Phthalates and System Interference by Using Liquid Chromatography/Tandem Mass Sectrometry[J].Flavour Fragrance Cosmetics,2013(5):36-42. |
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| Authors: | XIA Chunlan REN Ju ZHU Xiaomei CHENG Tianrong |
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| Affiliation: | (Huabao Food Flavor ＆ Fragrance Co. , Ltd. , Shanghai 201821, China) |
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| Abstract: | A method for determination of the phthalates by triple quadrupole UPLC-MS/MS had been developed. The effects of mobile phase, column packing etc. on the separation of target components were investigated, and the effect of system interference and solutions were also explored, thus it made possible to establish a method for determination of phthalates by LC- MS/MS. |
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| Keywords: | liquid chromatography/tandem mass spectrometry phthalate esters （PAEs） quantitative determination |
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