| 微波控制下咪唑类离子液体的制备 |
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| 引用本文： | 高转转,郭宪英.微波控制下咪唑类离子液体的制备[J].应用化工,2008,37(12). |
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| 作者姓名： | 高转转 郭宪英 |
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| 作者单位： | 1. 青岛大学,化学化工与环境学院,山东,青岛,266071
2. 青岛大学,化学化工与环境学院,山东,青岛,266071;东华大学,国家重点实验室,上海,200051 |
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| 基金项目： | 国家纤维材料改性重点实验室资助项目
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| 摘 要： | 以N-甲基咪唑和氯代正丁烷为原料在微波控制下合成了离子液体1-丁基-3-甲基咪唑氯盐(BMIm]Cl),对产物的结构作了红外光谱、核磁共振等分析。用该离子液体溶解纤维素,溶解度良好,并对溶解前后纤维素的结构变化、溶解机理进行了研究。
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| 关 键 词： | 离子液体 制备 纤维素 |
Preparation of N,N'-dialkylimidazolium based ionic liquids |
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| GAO Zhuan-zhuan,GUO Xian-ying.Preparation of N,N''''-dialkylimidazolium based ionic liquids[J].Applied chemical industry,2008,37(12). |
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| Authors: | GAO Zhuan-zhuan GUO Xian-ying |
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| Affiliation: | GAO Zhuan-zhuan1,GUO Xian-ying1,2 |
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| Abstract: | Ionic liquids of 1-butyl-3-methylimidazolium chloride was synthesized from 1-methyimidazole and 1-chlorobutane in microwave oven.The structure of the ionic liquids was characterized and analyzed by FTIR and 1H NMR.The ionic liquids to be used as solvent dissolved cellulose,it has good stability,and also study the structure of cellulose before and after dissolved,as well as dissolved mechanism. |
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| Keywords: | ionic liquids preparation cellulose |
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