| 3—甲基—4—吗啉基苯基重氮四氯化锡复盐的合成与表征 |
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| 引用本文： | 唐有根,蒋金芝.3—甲基—4—吗啉基苯基重氮四氯化锡复盐的合成与表征[J].化学试剂,1999,21(1):15-16,41. |
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| 作者姓名： | 唐有根 蒋金芝 |
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| 作者单位： | 中南工业大学化学系 |
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| 摘 要： | 以２－甲基－４－硝基苯胺为起始原料，合成了一种新的重氮光敏试剂３－甲基－４－吗啉基苯基重氮四氯化锡复盐，通过ＵＶ，ＩＲ，＾１ＨＮＭＲ和元素分析等手段对标题化合物及两个中间产物进行了结构表征。
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| 关 键 词： | 重氮盐 光敏试剂 合成 重氮四氯化锡 感光材料 |
Synthesis and characterization of 3 methyl 4 morpholinophenyl diazonium stannic chloride
double salt |
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| Abstract: | The new diazo photo sensitive
reagent, 3 methyl 4 morpholinophenyl diazonium stannic chloride double salt, was synthesized
by diazotisation, chlorination, reduction and diazotisation salification with 2 methyl 4
nitroaniline. The title compound and two intermediate products were identified by means of UV, IR,
1HNMR and elemental analysis, etc. |
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| Keywords: | diazonium salt photo sensitive reagent synthesis characterization |
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