| 微波快速合成1,4-萘醌 |
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| 引用本文： | 张前军,杨小生,赵超,朱海燕.微波快速合成1,4-萘醌[J].化学试剂,2006,28(3):183-184. |
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| 作者姓名： | 张前军 杨小生 赵超 朱海燕 |
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| 作者单位： | 1. 贵州省、中国科学院天然产物化学重点实验室,贵州,贵阳,550002;贵州大学,精细化工中心,贵州,贵阳,550025
2. 贵州省、中国科学院天然产物化学重点实验室,贵州,贵阳,550002 |
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| 摘 要： | 用微波辐射氧化1-萘酚合成1,4-萘醌,最佳反应条件是:HAc用量0.4mL,H2O2用量0.6mL,反应时间2min,微波功率280W,产率为50.9%。
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| 关 键 词： | 微波 1 4-萘醌 1-萘酚 合成 |
| 文章编号： | 0258-3283（2006）03-0183-02 |
| 收稿时间： | 2005-07-03 |
| 修稿时间： | 2005-07-03 |
Rapid synthesis of 1,4-naphthaqinone under microwave irradiation |
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| ZHANG Qian-jun,YANG Xiao-sheng,ZHAO Chao,ZHU Hai-yan.Rapid synthesis of 1,4-naphthaqinone under microwave irradiation[J].Chemical Reagents,2006,28(3):183-184. |
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| Authors: | ZHANG Qian-jun YANG Xiao-sheng ZHAO Chao ZHU Hai-yan |
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| Affiliation: | 1. The Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Sciences, Guiyang 550002, China; 2. Research and Development Center of Fine Chemicals, Guizhou Univerisity, Guiyang 550025,China |
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| Abstract: | 1,4-Naphthaqinone was prepared from 1-naphthol under microwave irradiation.The influences of solvent,time,microwave power and ratio of raw materials on the yield of the product were studied.The experimental result showed that the optimum conditions were as follows:HAc 0.4mL,H_2O_2 0.6mL,reaction time 2min,microwave power 280W,the yield was 50.9%. |
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| Keywords: | microwave irradiation 1-naphthol 1 4-naphthaqinone synthesis |
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