| 黄曲霉毒素饲料基体标准物质研究 |
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| 引用本文： | 赵天天,张伟,王秀嫔,李培武,张奇,马飞,张文.黄曲霉毒素饲料基体标准物质研究[J].化学试剂,2019(4):343-347. |
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| 作者姓名： | 赵天天 张伟 王秀嫔 李培武 张奇 马飞 张文 |
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| 作者单位： | 中国农业科学院油料作物研究所农业部油料作物生物学与遗传育种重点实验室;中国农业科学院油料作物研究所农业部生物毒素检测重点实验室;中国农业科学院油料作物研究所农业部油料产品质量安全风险评估实验室;中国农业科学院油料作物研究所农业部油料及制品质量监督检验测试中心;中国农业科学院油料作物研究所国家农业检测基准实验室(生物毒素) |
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| 基金项目： | 国家重点研发计划基金项目(2016YFF0201106);湖北省技术创新专项重大项目(2018ABA081);湖北省自然科学基金项目(2017CFB421) |
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| 摘 要： | 建立了含黄曲霉毒素B1、B2、G1、G2的饲料基体标准样品制备、定值和不确定度评估方法。饲料样品经加标、干燥、辐照灭菌、混匀、分装、密封制备而得。经过均匀性检验、稳定性检验、实验室联合定值以及不确定度评估等过程,最终确定饲料中黄曲霉毒素B1、B2、G1、G2的量值分别为(71. 23±1. 60)、(75. 53±1. 28)、(74. 87±1. 79)、(75. 77±2. 68)μg/kg。结果表明,饲料基体标准物质的均匀性良好,稳定性符合标准物质技术要求,同时分析并评估了该基体标准物质研制过程中引入的不确定度。该样品可用于饲料样品中黄曲霉毒素B1、B2、G1、G2的定性和定量检测。
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| 关 键 词： | 基体标准物质 黄曲霉毒素 联合定值 不确定度 |
Study on Matrix Reference Material for Aflatoxins in Feed |
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| ZHAO Tian-tian,ZHANG Wei,WANG Xiu-pin,LI Pei-wu,ZHANG Qi,MA Fei,ZHANG Wen.Study on Matrix Reference Material for Aflatoxins in Feed[J].Chemical Reagents,2019(4):343-347. |
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| Authors: | ZHAO Tian-tian ZHANG Wei WANG Xiu-pin LI Pei-wu ZHANG Qi MA Fei ZHANG Wen |
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| Affiliation: | (Key Laboratory of Biology and Genetic Improvement of Oil Crops,Ministry of Agriculture,Oil Crops Research Institute,Chinese Academy of Agricultural Sciences,Wuhan 430062,China;Key Laboratory of Detection for Mycotoxins,Ministry of Agriculture,Oil Crops Research Institute,Chinese Academy of Agricultural Sciences,Wuhan 430062,China;Laboratory of Risk Assessment for Oilseeds Products,Ministry of Agriculture,Oil Crops Research Institute,Chinese Academy of Agricultural Sciences,Wuhan 430062,China;Quality Inspection and Test Center for Oilseeds Products,Ministry of Agriculture,Oil Crops Research Institute,Chinese Academy of Agricultural Sciences,Wuhan 430062,China;National Standard Laboratory for Agricultural Testing (Mycotoxins),Oil Crops Research Institute,Chinese Academy of Agricultural Sciences,Wuhan 430062,China) |
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| Abstract: | ZHAO Tian-tian;ZHANG Wei;WANG Xiu-pin;LI Pei-wu;ZHANG Qi;MA Fei;ZHANG Wen(Key Laboratory of Biology and Genetic Improvement of Oil Crops,Ministry of Agriculture,Oil Crops Research Institute,Chinese Academy of Agricultural Sciences,Wuhan 430062,China;Key Laboratory of Detection for Mycotoxins,Ministry of Agriculture,Oil Crops Research Institute,Chinese Academy of Agricultural Sciences,Wuhan 430062,China;Laboratory of Risk Assessment for Oilseeds Products,Ministry of Agriculture,Oil Crops Research Institute,Chinese Academy of Agricultural Sciences,Wuhan 430062,China;Quality Inspection and Test Center for Oilseeds Products,Ministry of Agriculture,Oil Crops Research Institute,Chinese Academy of Agricultural Sciences,Wuhan 430062,China;National Standard Laboratory for Agricultural Testing (Mycotoxins),Oil Crops Research Institute,Chinese Academy of Agricultural Sciences,Wuhan 430062,China) |
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| Keywords: | matrix reference material Aflatoxin Joint determination uncertainty |
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