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| 诺卜醇及其衍生物的合成与表征 | |
| 引用本文： | 王宗德,肖转泉,陈金珠.诺卜醇及其衍生物的合成与表征[J].化学世界,2004,45(2):89-92. |
| 作者姓名： | 王宗德 肖转泉 陈金珠 |
| 作者单位： | 1. 江西农业大学林学院,江西,南昌,330045 2. 江西师范大学化学学院,江西,南昌,330027 3. 江西农业大学理学院,江西,南昌,330045 |
| 基金项目： | 国家自然科学基金资助项目(30060085);江西省自然科学基金项目(982019) |
| 摘 要： | 用压热法由β-蒎烯与多聚甲醛合成了诺卜醇;用相转移催化法合成了诺卜醇的乙基醚、丙基醚、丁基醚、戊基醚和苄基醚;由诺卜醇与酸酐反应合成了乙酸诺卜酯和丙酸诺卜酯。它们都具有较好的香气性质。所有产物的结构均用IR,MS,1HNMR及13CNMR分析进行了表征。 |
| 关 键 词： | β-蒎烯 诺卜醇 衍生物 合成 表征 |
| 文章编号： | 0367-6358(2004)02-0089-04 |
Synthesis and Identification of Nopol and Its Derivatives |
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| WANG Zong-de,XIAO Zhuan-quan,CHEN Jin-zhu.Synthesis and Identification of Nopol and Its Derivatives[J].Chemical World,2004,45(2):89-92. | |
| Authors: | WANG Zong-de XIAO Zhuan-quan CHEN Jin-zhu |
| Affiliation: | WANG Zong-de~1,XIAO Zhuan-quan~2,CHEN Jin-zhu~3 |
| Abstract: | Nopol was synthesized from β-pinene and formaldehyde by autoclave reaction. Nopyl ethyl ether, nopyl n-propyl ether, nopyl n-butyl ether, nopyl n-pentyl ether and nopyl benzyl ether were synthesized using phase transfer catalyst, nopyl propanoate and nopyl acetate were synthesized from the reaction of nopol and acid anhydride. All the compounds have good fragrant characteristics and have been identified by IR, MS, ()~1H NMR and ()~(13)C NMR. |
| Keywords: | β-pinene nopol derivative synthesis identification |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |