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中温酸性纳米化学复合镀Ni-P-ZrO2的研究
引用本文:刘胜宾,崔霞,李光明,梁臻,蔺万峰,邹建平.中温酸性纳米化学复合镀Ni-P-ZrO2的研究[J].电镀与涂饰,2010,29(6).
作者姓名:刘胜宾  崔霞  李光明  梁臻  蔺万峰  邹建平
作者单位:南昌航空大学环境与化学工程学院,江西,南昌,330063;南昌航空大学环境与化学工程学院,江西,南昌,330063;南昌航空大学环境与化学工程学院,江西,南昌,330063;南昌航空大学环境与化学工程学院,江西,南昌,330063;南昌航空大学环境与化学工程学院,江西,南昌,330063;南昌航空大学环境与化学工程学院,江西,南昌,330063
摘    要:研究了中温酸性环境下影响化学复合镀Ni-P-ZrO2工艺的主要因素,通过实验探索了ZrO2纳米颗粒的用量、搅拌速率、pH和温度对镀液及镀层性能的影响.获得了最佳工艺如下:ZrO2粒子用量30 mg/L,pH=5,搅拌速率500 r/min.在此工艺下所得镀层的显微硬度为650 HV,与Ni-P合金镀层的相对耐磨性为4.6,耐硝酸点蚀时间大于150 s,镀层磷含量为6.80%,ZrO2含量为17.6%.

关 键 词:化学复合镀  镍磷合金  二氧化锆  中温  酸性

Research on middle temperature acidic electroless nanocomposite plating of Ni-P-ZrO_2
LIU Sheng-bin,CUI Xia,LI Guang-ming,LIANG Zhen,LIN Wan-feng,ZOU Jian-ping.Research on middle temperature acidic electroless nanocomposite plating of Ni-P-ZrO_2[J].Electroplating & Finishing,2010,29(6).
Authors:LIU Sheng-bin  CUI Xia  LI Guang-ming  LIANG Zhen  LIN Wan-feng  ZOU Jian-ping
Affiliation:LIU Sheng-bin,CUI Xia,LI Guang-ming,LIANG Zhen,LIN Wan-feng,ZOU Jian-ping School of Environmental , Chemical Engineering,Nanchang Hangkong University,Nanchang 330063,China
Abstract:The influence of major factors on electroless composite plating process of Ni-P-ZrO_2 under middle temperature and acidic conditions was studied,and the effects of dosage of nano-ZrO_2 particles,stirring rate,pH and temperature on the properties of the bath and deposit were explored experimentally.The optimal process parameters were obtained as follows:dosage of ZrO_2 particle 30 mg/L, pH = 5 and stirring rate 500 r/min.The deposit obtained by this process has a microhardness 650 HV,relative wear-resistance...
Keywords:electroless composite plating  nickel-phosphorus alloy  zirconia  middle temperature  acidity  
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