| 嘧螨酯的合成与杀螨活性 |
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| 引用本文： | 刘若霖,张金波,李淼,张弘,刘长令.嘧螨酯的合成与杀螨活性[J].农药,2009,48(3). |
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| 作者姓名： | 刘若霖 张金波 李淼 张弘 刘长令 |
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| 作者单位： | 1. 辽宁大学,沈阳,110036;沈阳化工研究院,沈阳,110021
2. 沈阳化工研究院,沈阳,110021 |
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| 摘 要： | 以氰胺和异丙醇制备异丙氧基脒甲烷磺酸盐,再与三氟乙酰乙酸乙酯反应制得2-异丙氧基-4-羟基-6-三氟甲基嘧啶,最后与(E)-2-12-(氯甲基)苯基]3-甲氧基丙烯酸甲酯反应合成目标产物嘧螨酯,其结构经核磁、红外验证.生物活性测定结果表明该化合物具有良好的杀螨活性.
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| 关 键 词： | 嘧螨酯 合成 杀螨活性 |
Synthesis of Fluacrypyrim and Its Acaricidal Activity |
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| LIU Ruo-lin,ZHANG Jin-bo,LI Miao,ZHANG Hong,LIU Chang-ling.Synthesis of Fluacrypyrim and Its Acaricidal Activity[J].Pesticides,2009,48(3). |
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| Authors: | LIU Ruo-lin ZHANG Jin-bo LI Miao ZHANG Hong LIU Chang-ling |
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| Affiliation: | 1.Liaoning University;Shenyang 110036;China;2.Shenyang Research Institute of Chemical Industry;Shenyang 110021;China |
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| Abstract: | Fluacrypyrim was synthesized by reacting (E)-methyl 2-(2-(chloromethyl)phenyl)-3-methoxyacrylate with 2-isopropoxy-6-(trifluoromethyl)pyrimidin-4-ol prepared from ethyl 4,4,4-trifluoro-3-oxobutanoate and isopropyl carbamimidate methanesulfonate prepared from cyanamide and propan-2-ol, and its structure was confirmed by 1H NMR and IR. The biological test results show that fluacrypyrim has good acaricidal activity. |
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| Keywords: | fluacrypyrim synthesis acaricidal activity |
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