| 苦参总碱不同提取方法的比较 |
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| 引用本文： | 张玉芬,纪明山,张良,李海锋,王英姿.苦参总碱不同提取方法的比较[J].农药,2004,43(11):501-503. |
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| 作者姓名： | 张玉芬 纪明山 张良 李海锋 王英姿 |
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| 作者单位： | 1. 沈阳农业大学植物保护学院农药科学系,沈阳,110161
2. 沈阳农业大学分析测试中心,沈阳,110161 |
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| 基金项目： | 辽宁省十五攻关，项目名称:生物农药,生物制剂研制开发,项目编号:2001208001 |
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| 摘 要： | 对乙醇法、氨-氯仿法、树脂法提取的苦参总碱，用气相色谱法对有效成分进行分析和定量，比较了3种不同提取方法所提苦参总碱的纯度。测得树脂法提取的苦参总碱纯度是85．48％，高于其它两种方法，苦参总碱的相对标准偏差和回收率分别为1．82％和963％。结果表明树脂法是最佳提取方法。
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| 关 键 词： | 乙醇法 氨-氯仿法 树脂法 苦参总碱 气相色谱 |
| 文章编号： | 1006-0413(2004)11-501-03 |
The Comparison of Different Alkaloid Extraction Methods |
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| ZHANG Yu-Fen,JI Ming-Shan,ZHANG Liang,LI Hai-Feng,WANG Ying-Zi.The Comparison of Different Alkaloid Extraction Methods[J].Pesticides,2004,43(11):501-503. |
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| Authors: | ZHANG Yu-Fen JI Ming-Shan ZHANG Liang LI Hai-Feng WANG Ying-Zi |
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| Affiliation: | ZHANG Yu-Fen1,JI Ming-Shan1,ZHANG Liang1,LI Hai-Feng2,WANG Ying-Zi1 |
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| Abstract: | This paper used GC method for quantitative determination of alkaloids content from Sophora flavescentsextracted by ethanol method, chloroform method or resin method, comparing three different extraction methods. Thealkaloids content extracted by resin were 85.48%, higher than the other two methods, the relative standard deviationsand average recovery were 1.82% and 96.3%, respectively. The result indicated that resin method was optimalextraction method. |
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| Keywords: | ethanol method chloroform method resin method alkaloid GC |
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