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Processing and characterization of nano-magnetic Co0.5Ni0.5Fe2O4 system
Affiliation:1. Physical Chemistry Department, Laboratory of Surface Chemistry and Catalysis, National Research Center, Dokki, Cairo, Egypt;2. Zoology Department, College of Science, King Saud University, Riyadh 11451, Kingdom of Saudi Arabia;3. Electron Microscope and Thin Films Department, National Research Center (NRC), El- Behooth Street, Giza 12622, Egypt;1. Department of Environmental Engineering, Konkuk University, Seoul 143-701, Korea;2. Green Technology Co., Ltd., 6F Hanam Venture Tower B/D, ChangWoo-Dong, HaNam-Si 465-120, GyeongGi-Do, Korea;3. Department of Advanced Technology Fusion, Konkuk University, Seoul 143-701, Korea;1. Department of Chemical Engineering, School of Chemical and Petroleum Engineering, Shiraz University, Shiraz 71345, Iran;2. Gas Center of Excellence, Shiraz University, Shiraz 71345, Iran;1. Department of Physics, Bahauddin Zakariya University, Multan 60800 Pakistan;2. Department of Physics, Islamia University, Bahawalpur 63100 Pakistan;3. Nust College of Electrical and Mechanical Engineering, Islamabad, Pakistan;1. Department of Chemical Engineering, Kwangwoon University, Seoul 139-701, Republic of Korea;2. National Institute of Environmental Research, Incheon 404-708, Republic of Korea;3. Department of Chemistry, Sultan Qaboos University, Muscat 123, Oman;1. Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, P.O. Box 87317-51167, Iran;2. Institute of Nano Science and Nano Technology, University of Kashan, Kashan, P.O. Box 87317-51167, Iran
Abstract:Various techniques such as X-ray diffraction (XRD), infrared (IR) spectroscopy, scanning electron micrographs (SEM), energy dispersive X-ray (EDX) and a vibrating sample magnetometer (VSM) were used to investigate the structural, morphological, and magnetic properties of spinel Co0.5Ni0.5Fe2O4 system. XRD and IR analyses enabled us to determine the functional group and structural parameters of Co0.5Ni0.5Fe2O4. EDX measurements showed the concentrations of O, Ni, Fe, and Co species involved in Co0.5Ni0.5Fe2O4 specimen from the uppermost surface to the bulk layers. The magnetization and coercivity of the as synthesized composite were 77 emu/g and 128 Oe, respectively.
Keywords:XRD  SEM  EDX  VSM  Crystallite size
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