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| 乙二胺-水体系中合成氧化锌纳米带 | |
| 引用本文： | 姜妲,翟玉春,陈元涛,龚睿,张炜.乙二胺-水体系中合成氧化锌纳米带[J].过程工程学报,2006,6(5):841-844. |
| 作者姓名： | 姜妲 翟玉春 陈元涛 龚睿 张炜 |
| 作者单位： | 1. 东北大学材料与冶金学院,辽宁,沈阳,110004 2. 青海师范大学化学系,青海,西宁,810008 3. 兰州大学化学化工学院,甘肃,兰州,730000 |
| 基金项目： | 国家高技术研究发展计划(863计划) |
| 摘 要： | 以乙二胺为介质,采用溶剂热法,在乙二胺-水体系中合成出宽度为20~30 nm、长度为500~600 nm的氧化锌纳米带,并进行了表征. 在反应过程中,氧化锌纳米带通过"溶解-结晶"机制形成,溶剂乙二胺的配位是氧化锌纳米带形成的关键因素,通过调整NaOH用量控制溶液碱度,实现了氧化锌纳米带的取向生长. |
| 关 键 词： | 氧化锌 纳米带 乙二胺 溶剂热合成 |
| 文章编号： | 1009-606X（2006）05-0841-04 |
| 收稿时间： | 2005-12-05 |
| 修稿时间： | 2006-01-09 |
Synthesis of Zinc Oxide Nanobelts in Aqueous Solution of Ethylene Diamine |
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| JIANG Da,ZHAI Yu-chun,CHEN Yuan-tao,GONG Rui,ZHANG Wei.Synthesis of Zinc Oxide Nanobelts in Aqueous Solution of Ethylene Diamine[J].Chinese Journal of Process Engineering,2006,6(5):841-844. | |
| Authors: | JIANG Da ZHAI Yu-chun CHEN Yuan-tao GONG Rui ZHANG Wei |
| Affiliation: | 1. School of Materials and Metallurgy, Northeastern University, Shenyang, Liaoning 110004, China; 2. Department of Chemistry, Qinghai Normal University, Xining, Qinghai 810008, China; 3. School of Chemistry and Technology, Lanzhou University, Lanzhou, Gansu 730000, China |
| Abstract: | Zinc oxide nanobelts were synthesized in aqueous solution of ethylene diamine by solvothermal synthesis and characterized at the same time. The width and length of zinc oxide nanobelts are 20-30 nm and 500-600 nm respectively. Zinc oxide nanobelts were prepared through dissolution-crystallization mechanism. Ethylene diamine bonding was a key factor in synthesis of zinc oxide nanobelts, and the oriented growth of zinc oxide was controlled by the quantity of sodium hydroxide. |
| Keywords: | zinc oxide nanobelts ethylene diamine solvothermal synthesis |
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