| 环【8】吡咯及其衍生物的一锅法合成、表征及光谱分析 |
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| 引用本文： | 陈芳军,黄可龙,徐海,许慧.环【8】吡咯及其衍生物的一锅法合成、表征及光谱分析[J].广州化工,2009,37(1):61-64. |
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| 作者姓名： | 陈芳军 黄可龙 徐海 许慧 |
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| 作者单位： | 中南大学化学化工学院,湖南,长沙,410083 |
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| 摘 要： | 一锅法合成了环【8】吡咯及其衍生物环【6]吡咯和环7】吡咯，用正交实验获得了合成的最佳条件，使产率分别达到32％，20％，9％，对三个化合物进行了核磁共振氢谱、核磁共振碳谱、元素分析表征，研究了环n】吡咯（n=6，7，8）的紫外可见吸收光谱和荧光发射光谱。
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| 关 键 词： | 环 吡咯(n=6 7 8) 合成与表证 紫外可见光谱 荧光光谱 |
One-Spot Method Synthesis and Characterization and Spectrum Analysis of Cyclo[8]pyrrole and its Derivatives |
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| CHEN Fang-jun,HUANG Ke-long,XU Hai,XU Hui.One-Spot Method Synthesis and Characterization and Spectrum Analysis of Cyclo[8]pyrrole and its Derivatives[J].GuangZhou Chemical Industry and Technology,2009,37(1):61-64. |
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| Authors: | CHEN Fang-jun HUANG Ke-long XU Hai XU Hui |
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| Affiliation: | School of Chemistry and Chemical Engineering;Central South University;Hunan Changsha 410083;China |
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| Abstract: | Cyclo8]pyrrole and its two derivatives(cylo6]pyrrole and cyclo7]pyrrole) were synthesized by one spot method.The optimum processing conditions were found in orthogonal experiments,bringing the yields were 32 %,20 %,9 %,respectively.The structures of the three compounds were characterized by 1HNMR,13 C NMR and elemental analysis.The UV-vis spectrums and fluorescence spectrums of the three compounds were studied. |
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| Keywords: | cyclo pyrrole （n=6 7 8） synthesis and characterization UV-vis spectrums fluorescence spectrums |
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