| 酯交换法合成碳酸甲乙酯工艺研究 |
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| 引用本文： | 王桂珍,方诒胜.酯交换法合成碳酸甲乙酯工艺研究[J].广州化工,2012,40(16):101-102,129. |
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| 作者姓名： | 王桂珍 方诒胜 |
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| 作者单位： | 铜陵金泰化工股份有限公司,安徽铜陵,244000 |
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| 摘 要： | 以MgO/SiO2复合催化剂用于碳酸二甲酯与碳酸二乙酯酯交换合成碳酸甲乙酯反应,对其合成工艺进行了初步研究。通过正交实验得出最佳合成工艺条件。在最佳条件下进行验证,产物的收率最高可以达到61.02%且重复性好。
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| 关 键 词： | 碳酸甲乙酯 碳酸二甲酯 碳酸二乙酯 酯交换法 |
Study on the Synthesis of Methyl Ethyl Carbonate by Transesterification |
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| WANG Gui-zhen,FANG Yi-sheng.Study on the Synthesis of Methyl Ethyl Carbonate by Transesterification[J].GuangZhou Chemical Industry and Technology,2012,40(16):101-102,129. |
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| Authors: | WANG Gui-zhen FANG Yi-sheng |
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| Affiliation: | WANG Gui - zhen, FANG Yi - sheng (Tongling Jintai Hemical Industrual Co. , Ltd. , Anhui Tongling 244000, China) |
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| Abstract: | The dimethyl carbonate and diethyl carbonate as raw materials, MgO/SiO2 as composite catalyst, methyl ethyl carbonate was synthesized, and a preliminary stuty on technological conditions for synthesis was carried out. The optimum conditions were obtained through orthogonal experiment. Under optimal conditions of verification, product yield can reach 61.02% and had good repeatability. |
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| Keywords: | methyl ethyl carbonate dimethyl carbonate diethyl carbonate transesterification |
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