| KIT-6新型介孔分子筛的合成与表征 |
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| 引用本文： | 李旭日,李瑞生.KIT-6新型介孔分子筛的合成与表征[J].河南化工,2012(13):35-37. |
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| 作者姓名： | 李旭日 李瑞生 |
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| 作者单位： | 1. 沈阳化工大学材料科学与工程学院,辽宁沈阳,110142
2. PPG涂料天津有限公司,天津,300000 |
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| 摘 要： | 以P123为模板剂，正硅酸乙酯为硅源，采用水解法制备了介孔分子筛KIT-6，通过X射线衍射、傅立叶红外检测、N2吸附脱附、扫描电子显微镜对样品进行表征，结果表明该样品具有Ia3d立方相介孔材料的有序特征，为弯曲的棒状形貌。其比表面积为813．7m2／g，孔径为8．2nm。
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| 关 键 词： | KIT-6 水解法 介孔材料 |
Synthesis and Characterization of KIT -6 Mesoporous Molecular sieve |
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| LI Xu-ri,LI Rui-sheng.Synthesis and Characterization of KIT -6 Mesoporous Molecular sieve[J].Henan Chemical Industry,2012(13):35-37. |
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| Authors: | LI Xu-ri LI Rui-sheng |
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| Affiliation: | 1.College of Materials Science and Engineering,Shenyang University of Chemical Technology,Shenyang 110142,China;2.PPG Coating(Tianjin) Co.Ltd,Tianjin 300000,China) |
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| Abstract: | Mesoporous molecular sieve KIT-6 are prepared by hybridization with P123 as template and ethyl silicate as silicon source.The samples are characterized by XRD,N2 adsorption-desorption measurements,SEM and FT-IR.The result indicates that the samples have Ia3d cubic mesoporous materials’ordered features and curved rod-like morphologies.Its specific surface area and pore size are 813.7 m2/g and 8.2 nm. |
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| Keywords: | KIT-6 hybridization mesoporous molecular sieve |
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