| 流化床CVD法原位合成CNTs-Ni-TiO2及其光催化性能 |
| |
| 引用本文： | 陆金东,陈爱平,马磊,何洪波,倪道克,李春忠.流化床CVD法原位合成CNTs-Ni-TiO2及其光催化性能[J].化工学报,2012,63(4):1070-1075. |
| |
| 作者姓名： | 陆金东 陈爱平 马磊 何洪波 倪道克 李春忠 |
| |
| 作者单位： | 华东理工大学材料科学与工程学院，超细材料制备与应用教育部重点实验室，上海 200237 |
| |
| 基金项目： | 国家自然科学基金项目(20925621);上海市科委纳米专项(1052nm02400)~~ |
| |
| 摘 要： | 采用柠檬酸修饰溶胶-凝胶法制备NiO-TiO2催化剂，然后于流化床反应器中直接在NiO-TiO2表面原位生长多壁碳纳米管，制备出CNTs-Ni-TiO2复合光催化剂。采用XRD、SEM、TG、BET、PL荧光光谱等方法对制备的样品进行了表征，以亚甲基蓝降解为模型反应，考察了复合催化剂在紫外线下的光催化性能。结果表明，在NiO含量为5%的NiO-TiO2催化剂上生长CNTs后得到的CNTs-Ni-TiO2复合材料具有较高的光催化活性。
|
| 关 键 词： | 溶胶-凝胶法 流化床 CNTs 光催化 TiO2 化学气相沉积 |
| 收稿时间： | 2011-09-13 |
| 修稿时间： | 2012-01-04 |
Synthesis of CNTs-Ni-TiO2 nanocomposites by in-situ fluidized bed CVD and its photocatalytic activity |
| |
| LU Jindong
,
CHEN Aiping
,
MA Lei
,
HE Hongbo
,
NI Daoke
,
LI Chunzhong.Synthesis of CNTs-Ni-TiO2 nanocomposites by in-situ fluidized bed CVD and its photocatalytic activity[J].Journal of Chemical Industry and Engineering(China),2012,63(4):1070-1075. |
| |
| Authors: | LU Jindong CHEN Aiping MA Lei HE Hongbo NI Daoke LI Chunzhong |
| |
| Affiliation: | Key Laboratory for Ultrafine Materials of Ministry of Education, School of Material Science and Engineering,East China University of Science and Technology, Shanghai 200237,China |
| |
| Abstract: | NiO-TiO2 catalyst was prepared with the modified citric acid sol-gel method.Carbon nanotubes(CNTs)was directly grown on the surface of the NiO-TiO2 by fluidized bed chemical vapor deposition(CVD).The prepared CNTs-Ni-TiO2 nanocomposite photocatalysts were characterized by XRD,SEM,TG,BET and PL.The photocatalytic performance of CNTs-Ni-TiO2 was evaluated by degradation of methylene blue under UV light.The results indicated that CNTs-Ni-TiO2 nanocomposite showed the highest degradation activity when the dosage of NiO was 5%. |
| |
| Keywords: | sol-gel fluidized bed CNTs photocatalysis TiO2 chemical vapor deposition |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
| 点击此处可从《化工学报》浏览原始摘要信息 |
|
点击此处可从《化工学报》下载全文 |
