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SAFE与SDE法对金华火腿皮下脂肪气味活性物质研究
引用本文:刘笑生,刘建斌,刘梦雅,何聪聪,杨政茂,宋焕禄.SAFE与SDE法对金华火腿皮下脂肪气味活性物质研究[J].北京轻工业学院学报,2014(1):40-46.
作者姓名:刘笑生  刘建斌  刘梦雅  何聪聪  杨政茂  宋焕禄
作者单位:北京工商大学分子感官科学实验室,北京100048
基金项目:“十二五”农村领域国家科技计划项目(2011AA100805-0-3).
摘    要:通过溶剂辅助风味蒸发系统(SAFE)和同时蒸馏提取技术(SDE)与气相色谱-嗅闻仪-质谱联机法(GC-O-MS)结合,对已发酵18个月的金华火腿皮下脂肪气味化合物进行定性定量分析和感官评价.SAFE和SDE法分别检测并嗅闻到40种和22种气味活性化合物,对脂肪气味贡献度较大的10种关键性化合物分别是:己醛、庚醛、二异丙基二硫醚、辛醛、反-2-辛烯醛、3-甲基丁酸、反,反-2,4-癸二烯醛、γ-癸内酯、γ-十一内酯和苯乙酸.

关 键 词:SAFE  SDE  金华火腿皮下脂肪  气味活性物质

Study on Odorants in Subcutaneous Fat of Jinhua Ham by SAFE and SDE Methods
LIU Xiao-sheng,LIU Jian-bin,LIU Meng-ya,HE Cong-cong,YANG Zheng-mao,SONG Huan-lu.Study on Odorants in Subcutaneous Fat of Jinhua Ham by SAFE and SDE Methods[J].Journal of Beijing Institute of Light Industry,2014(1):40-46.
Authors:LIU Xiao-sheng  LIU Jian-bin  LIU Meng-ya  HE Cong-cong  YANG Zheng-mao  SONG Huan-lu
Affiliation:*(Laboratory of Molecular Sensory Science, Beifing Technology and Business University, Beifing 100048, China)
Abstract:The odor active compounds in subcutaneous fat of Jinhua ham fermented for 18 months were extracted by solvent-assisted flavorevaporation (SAFE) and simultaneous distillation extraction (SDE) methods and analyzed by gas chromatography-Olfactrometry-mass spectrometry (GC-O-MS). Totally 40 odorants were detected by SAFE while 22 odorants were detected by SDE. About 10 odorants were identi- fled as key odor active compounds, which were hexanal, heptanal, isopropyl disulfide, octanal, (E)-2-octenal, 3-methylbutanoic acid, ( E, E) -2,4-decadienal, γ-decalactone, and γ-undecalactone.
Keywords:solvent-assisted flavourevaporation  simultaneous distillation extraction  subcutaneous fat ofJinhua ham  odor active compounds
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