| 中孔分子筛MCM-48的合成研究 |
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| 引用本文： | 张鑫,姜泽忠,等.中孔分子筛MCM-48的合成研究[J].北京服装学院学报,2001,21(2):34-39. |
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| 作者姓名： | 张鑫 姜泽忠 |
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| 作者单位： | 北京服装学院化工研究所，北京服装学院化工研究所，北京服装学院化工研究所 北京100029，北京100029，本院97级本科生，北京100029 |
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| 摘 要： | 本文比较系统地考察了模板剂用量，水用量，晶化时间，晶化温度等因素对合成中孔分子筛MCM－48的影响，并对Si-MCM-48的合成过程铝原子的引入作了初步探索，通过XRD，IRTG－DTA等测试手段对产物进行了表征。
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| 关 键 词： | 中孔分子筛 MCM－48 水热合成 表征 催化 中孔材料 模板剂用量 |
| 文章编号： | 1001-0564(2001)02-0034-06 |
Synthesis of Mesoporous Molecular Sieve MCM-48 |
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| Zhang Xin Jiang Zezhong Fu Jiquan Research Institute of Chemical Engineering,Beijing Institute of Clothing Technology,Beijing.Synthesis of Mesoporous Molecular Sieve MCM-48[J].Journal of Beijing Institute of Clothing Technology(Nature Science Edition),2001,21(2):34-39. |
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| Authors: | Zhang Xin Jiang Zezhong Fu Jiquan Research Institute of Chemical Engineering Beijing Institute of Clothing Technology Beijing |
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| Affiliation: | Zhang Xin Jiang Zezhong Fu Jiquan Research Institute of Chemical Engineering,Beijing Institute of Clothing Technology,Beijing 100029 |
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| Abstract: | Mesoporous molecular sieve MCM-48 was prepared hydrothermally with CTAB, NaOH, TEOS as raw materials. The effects of CTAB. H20, the crystallization time and the crystallization temperature on synthesis of mesoporous molecular sieve MCM- 48 were studied in detail. Further more. the synthesis of Al- Si- MCM- 48 was also studied with aluminum being the source. Characterization results obtained from the determination of XRD. JR spectrum and TG- DTA showed that the products possessed similar structure properties to those reported in literatures. At last, four conclusions were obtained. |
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| Keywords: | mesoporous molecular sieve MCM-48 characterization synthesis |
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