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锐钛矿型纳米TiO2的制备及其对甲基红的光催化降解
引用本文:严安,刘泽华,黄静.锐钛矿型纳米TiO2的制备及其对甲基红的光催化降解[J].天津轻工业学院学报,2009(4):45-48.
作者姓名:严安  刘泽华  黄静
作者单位:天津市制浆造纸重点实验室,天津科技大学材料科学与化学工程学院,天津300457
基金项目:国家自然科学基金资助项目(50503016)
摘    要:利用溶胶-凝胶法制备纳米级锐钛矿二氧化钛粉末,并用XRD、FTIR、SEM、AFM等手段对粉体的尺寸、微观形貌、结构和性能进行表征,考察该粉体对甲基红的催化氧化能力.结果表明:产物为锐钛矿型TiO2纳米粉末,其直径约为20nm;当甲基红的初始质量浓度为20mg/L,纳米TiO2投加量为0.7g/L时,经功率为8W、波长365nm的紫外灯照射30min后,甲基红降解率达到95.58%.

关 键 词:溶胶-凝胶法  二氧化钛  甲基红  光催化性能

Preparation of Anatase-Phase Nano-TiO2 and Photocatalytic Degradation of Methtl Red
YAN An,LIU Ze-hua,HUANG Jing.Preparation of Anatase-Phase Nano-TiO2 and Photocatalytic Degradation of Methtl Red[J].Journal of Tianjin University of Light Industry,2009(4):45-48.
Authors:YAN An  LIU Ze-hua  HUANG Jing
Affiliation:(Tianjin Key Laboratory of Pulp and Paper,College of Material Science and Chemical Engineering, Tianjin University of Science & Technology ,Tianjin 300457 ,China)
Abstract:The anatase TiO2 nano-power was prepared by the sol-gol method. The size,appearance,structure and property of TiO2 were analyzed by XRD,SEM,FTIR and AFM. The photocatalytic oxidation properties were examined by the degradation of methly red. The results show that the samples are anatase TiO2 particles with diameter of 20 nm. When the concentration of methyl red is 20 mg/L and the dosage of the powers is 0.7 g/L ,the degradation rate of methyl red is up to 95.58% after irradiated half an hour with the 8 W ultraviolet lamp with L=365 nm.
Keywords:sol-gol method  titanium dioxide  methyl red  photocatalytic capability
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