| Al掺杂ZnO超细粉体的制备及表征 |
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| 引用本文： | 黄杏芳,崔升,沈晓冬.Al掺杂ZnO超细粉体的制备及表征[J].福建建筑高等专科学校学报,2011(1):72-75. |
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| 作者姓名： | 黄杏芳 崔升 沈晓冬 |
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| 作者单位： | [1]福建工程学院材料科学与工程系,福建福州350108 [2]南京工业大学材料科学与工程学院,江苏南京210009 |
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| 摘 要： | 利用溶胶-凝胶法在一系列不同实验条件下制备出了ZAO超细粉体,用正交试验法对实验条件进行设计,确定了最佳实验条件,并利用差热-热重分析仪、X-射线衍射仪、扫描电镜等对得到的ZAO超细粉体进行了分析和表征。结果表明,在煅烧温度1 150℃,乙醇与水的比例为2.5,醋酸锌浓度为2.5 mol/L,柠檬酸三胺浓度为0.5 mol/L,氧化铝与氧化锌的质量比为3%的实验条件下,能够得到具有交错柱状晶体的ZAO超细粉体。同时,在850℃处成功对ZnO进行了铝的掺杂。
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| 关 键 词： | ZAO超细粉体 溶胶-凝胶法 正交试验 |
Preparation and characterization of AL adulterated ZnO super powders |
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| Huang Xingfang,Cui Sheng,Shen Xiaodong.Preparation and characterization of AL adulterated ZnO super powders[J].Journal of Fujian College of Architecture & C.E.,2011(1):72-75. |
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| Authors: | Huang Xingfang Cui Sheng Shen Xiaodong |
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| Affiliation: | 1.Materials Science and Engineering Department,Fujian University of Technology,Fuzhou 350108,China; 2.College of Material Science and Engineering,Nanjing University of Technology,Nanjing 210009,China) |
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| Abstract: | ZAO super powders were prepared by sol-gel method under different conditions.The optimum experimental condition was established by orthogonal design.The powders were analysed and characterized by TG-DSC,XRD,TEM.Under the condition of sinter temperature of 1150℃,ethanol： water is 2.5,（CH3COO）2Zn·2H2O concentration is 2.5mol/L,（NH4）3C6H5O7 concentration is 0.5mol/L,AlO：ZnO is 3%（in weight）,ZAO super powder with column crystals was obtained.And at 850℃,ZnO was adulterated by Al. |
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| Keywords: | ZAO super powder sol-gel method orthogonal design |
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