| Mg(OH)_2纳米片的制备与表征 |
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| 引用本文： | 宋彩霞,胡正水,傅洵.Mg(OH)_2纳米片的制备与表征[J].青岛科技大学学报,2009,30(3):200-202. |
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| 作者姓名： | 宋彩霞 胡正水 傅洵 |
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| 作者单位： | 宋彩霞,胡正水,SONG Cai-xia,HU Zheng-shui(青岛科技大学,材料科学与工程学院,山东,青岛,266042);傅洵,FU Xun(青岛科技大学,化学与分子工程学院,山东,青岛,266042)
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| 基金项目： | 山东省优秀中青年科学家科研奖励基金 |
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| 摘 要： | 以对硝基偶氮间苯二酚为表面修饰剂,将硫酸镁溶液与氢氧化钠溶液在80℃下直接反应,制备出片状的纳米氢氧化镁。所得样品用XRD,TEM和SEM等技术进行表征,考察了实验条件对样品形貌的影响。结果表明,氢氧化镁纳米片的直径为100~200nm、厚度15 nm左右,比表面积129 m2.g-1。初步讨论了Mg(OH)2片状纳米晶的生长机理。
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| 关 键 词： | Mg(OH)2 纳米片 表面修饰 |
Preparation and Characterization of Mg(OH)_2 Nanosheets |
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| SONG Cai-xiaa,HU Zheng-shuia,FU Xunb.Preparation and Characterization of Mg(OH)_2 Nanosheets[J].Journal of Qingdao University of Science and Technology:Natutral Science Edition,2009,30(3):200-202. |
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| Authors: | SONG Cai-xiaa HU Zheng-shuia FU Xunb |
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| Affiliation: | Qingdao University of Science and Technology a.College of Material Science and Engineering;b.College of Chemistry and Molecular Engineering;Qingdao 266042;China |
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| Abstract: | Mg(OH)2 nanosheets with size of 100~200 nm and thickness of 15 nm were prepared from the precipitation reaction between MgSO4 and NaOH at 80 ℃ using 4-(p-nitrophenylazo) resorcinol(NPR) as surface modifier.The products were characterized using XRD,TEM,and SEM.The influence of various experimental parameters on the morphologies of Mg(OH)2 nanosheets were investigated.The specific surface area was determined to be 129 m2·g-1.Possible growth mechanism of Mg(OH)2 nanosheets was discussed. |
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| Keywords: | Mg(OH)2 |
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