| q—CS/TEOS复合膜的制备及吸附性能的研究 |
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| 引用本文： | 王蕊,封瑞江,王吉林,敖敏.q—CS/TEOS复合膜的制备及吸附性能的研究[J].辽宁石油化工大学学报,2011,31(1):13-16,20. |
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| 作者姓名： | 王蕊 封瑞江 王吉林 敖敏 |
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| 作者单位： | 辽宁石油化工大学石油化工学院; |
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| 摘 要： | 以正硅酸乙酯为无机组分,季铵化壳聚糖为有机组分,通过溶胶-凝胶法制备一系列不同正硅酸乙酯质量分数的季铵化壳聚糖/正硅酸乙酯(q-CS/TEOS)复合阴离子交换膜.利用红外光谱分析(FT-IR)对膜的化学结构进行表征.另外,利用得到的杂化膜对水溶液中的Cr(Ⅵ)离子进行吸附性能考察.实验对吸附时间、体系pH值、溶液温度等...
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| 关 键 词： | 季铵化壳聚糖 正硅酸乙酯 复合膜 Cr(Ⅵ) 吸附 |
Preparation and Adsorption Performance of q-CS/TEOS Hybrid Membranes |
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| WANG Rui,FENG Rui-jiang,WANG Ji-lin,AO Min.Preparation and Adsorption Performance of q-CS/TEOS Hybrid Membranes[J].Journal of Liaoning University of Petroleum & Chemical Technology,2011,31(1):13-16,20. |
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| Authors: | WANG Rui FENG Rui-jiang WANG Ji-lin AO Min |
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| Affiliation: | WANG Rui,FENG Rui-jiang,WANG Ji-lin,AO Min(School of Petrochemical Technology,Liaoning Shihua University,Fushun Liaoning 113001,P.R.China)Received 17 July 2010,revised 1 November 2010,accepted 23 November 2010 |
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| Abstract: | A series of hybrid membranes composed of quaternized chitosan(q-CS) and tetraethoxysilane(TEOS) were prepared by sol-gel method,taking q-CS and the TEOS as organic and inorganic component respectively.The structure of the hybrid membranes was investigated by FT-IR.The adsorption performance of the membranes for Cr(Ⅵ) ions from aqueous solution was also studied.The effect of adsorption time,the pH value of solution and temperature of the adsorption on adsorption results were studied and show that the suitable membrane is composed of 38wt% TEOS,and the optimum adsorption conditions were carried out at 35 ℃ for 180 minutes with pH value of 5.0～8.0. |
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| Keywords: | Quaternized chitosan Tetraethoxysilane Hybrid membrane Cr(Ⅵ) Adsorption |
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