| 微波水热合成纳米孔金属磷酸盐CoVSB-1 |
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| 引用本文： | 解丽丽,王利军,袁 昊,田 震.微波水热合成纳米孔金属磷酸盐CoVSB-1[J].上海第二工业大学学报,2010,27(1):7-11. |
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| 作者姓名： | 解丽丽 王利军 袁 昊 田 震 |
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| 作者单位： | 上海第二工业大学城市建设与环境工程学院,上海,201209 |
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| 基金项目： | 国家自然科学基金，上海市教育发展基金会"晨光计划"基金 |
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| 摘 要： | 微波水热合成了纳米孔金属磷酸盐CoVSB-1，453K微波辐照30min产率可达89％。CoVSB-1的晶化时间缩短为传统水热晶化时间的1／8。快速结晶使CoVSB．1产物颗粒分布更均匀、长径比更小。VSB-1晶粒的生成至少需要微波水热晶化60min。
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| 关 键 词： | CoVSB-1 VSB-1 微波水热合成 |
Microwave-Hydrothermal Synthesis of Nanoporous Metal Phosphate CoVSB-1 |
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| XIE Li-li,WANG Li-jun,YUAN Hao,TIAN Zhen.Microwave-Hydrothermal Synthesis of Nanoporous Metal Phosphate CoVSB-1[J].Journal of Shanghai Second Polytechnic University,2010,27(1):7-11. |
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| Authors: | XIE Li-li WANG Li-jun YUAN Hao TIAN Zhen |
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| Affiliation: | XIE Li-li,WANG Li-jun,YUAN Hao,TIAN Zhen (School of Urban Development , Environmental Engineering,Shanghai Second Polytechnic University,Shanghai 201209,P.R.China) |
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| Abstract: | Nanoporous metal phosphate CoVSB-1 was prepared via the microwave-hydrothermal synthesis, and the yield of about 89 % has been achieved for 30 min at 453 K under microwave irradiation. The crystallization time of CoVSB-1 was reduced by about 8 times compared with the conventional electric heating. The fast crystallization favors more uniform particle size distribution and smaller aspect ratios of CoVSB-1 product. By the microwave-hydrothermal synthesis, the product of VSB-1 formed for at least 60 min. |
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| Keywords: | CoVSB-1 VSB-1 CoVSB-1 VSB-1 microwave-hydrothermal synthesis |
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