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| 高效液相色谱—电感耦合等离子体质谱法测定大米中无机砷方法研究 | |
| 引用本文： | 潘浩,李筱薇,宫智勇,吴永宁.高效液相色谱—电感耦合等离子体质谱法测定大米中无机砷方法研究[J].武汉工业学院学报,2012,31(3):1-5. |
| 作者姓名： | 潘浩 李筱薇 宫智勇 吴永宁 |
| 作者单位： | 1. 武汉工业学院食品科学与工程学院,湖北武汉430023;国家食品安全风险评估中心,北京100021 2. 国家食品安全风险评估中心,北京,100021 3. 武汉工业学院食品科学与工程学院,湖北武汉,430023 |
| 摘 要： | 针对SRM1568a标准参考物和实际大米样品比较不同浓度的三氟乙酸、盐酸、硝酸、醋酸溶液在热提取条件下对大米无机砷的提取效果,确定最佳提取酸,同时比较超声波提取、微波辅助提取与热提取的效果,确定最终提取方法. |
| 关 键 词： | ICP—MS 无机砷 大米 |
Inorganic arsenic determination study on rice using HPLC-ICP-MS |
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| PAN Hao , LI Xiao-wei , GONG Zhi-yong , WU Yong-ning.Inorganic arsenic determination study on rice using HPLC-ICP-MS[J].Journal of Wuhan Polytechnic University,2012,31(3):1-5. | |
| Authors: | PAN Hao LI Xiao-wei GONG Zhi-yong WU Yong-ning |
| Affiliation: | 1.School of Food Science and Engineering,Wuhan Polytechnic University,Wuhan 430023,China; 2.China National Centre of Food Safety Risk Assessment,Beijing,100021,China) |
| Abstract: | This paper aims at choosing the most efficient extraction acid during trifluoroacetic acid(TFA),hydrochloric acid,nitric acid,and acetic acid for rice inorganic arsenic extraction using heat extraction.SRM 1568a and real rice sample were used as analyte.Meanwhile,the extraction modes for ultrasonic and microwave were compared with heat extraction,then chose the best one. |
| Keywords: | ICP-MS inorganic arsenic rice |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |