| 自组装单层膜表面的Bi2Ti2O7薄膜制备与表征 |
| |
| 引用本文： | 夏傲,黄剑锋,谈国强.自组装单层膜表面的Bi2Ti2O7薄膜制备与表征[J].功能材料,2012,43(11):1403-1406. |
| |
| 作者姓名： | 夏傲 黄剑锋 谈国强 |
| |
| 作者单位： | 陕西科技大学教育部轻化工助剂化学与技术重点实验室,陕西西安,710021 |
| |
| 基金项目： | 国家青年科学基金资助项目，陕西省自然科学基金资助项目 |
| |
| 摘 要： | 以硝酸铋和钛酸四丁酯为原料,以三氯十八烷基硅烷(OTS)为模板,采用自组装单层膜(self-as-sembled monolayers,SAMs)技术,在玻璃基板上成功制备了Bi2Ti2O7晶态薄膜。借助X射线衍射(XRD)、场发射扫描电子显微镜(FE-SEM)、X射线能谱(EDS)及原子力显微镜(AFM)等测试手段对Bi2Ti2O7薄膜进行了表征。结果表明,以OTS为模板利用自组装技术,经540℃煅烧2h可成功制得立方相Bi2Ti2O7晶态薄膜,且薄膜表面平整光滑,均匀致密。
|
| 关 键 词： | 自组装单层膜 Bi2Ti2O7 薄膜 表征 |
Preparation and characterization of Bi2Ti2O7 thin film on self-assembled monolayer |
| |
| XIA Ao,HUANG Jian-feng,TAN Guo-qiang.Preparation and characterization of Bi2Ti2O7 thin film on self-assembled monolayer[J].Journal of Functional Materials,2012,43(11):1403-1406. |
| |
| Authors: | XIA Ao HUANG Jian-feng TAN Guo-qiang |
| |
| Affiliation: | (Key Laboratory of Auxiliary Chemistry & Technology for Chemical Industry,Ministry of Education,Shaanxi University of Science and Technology,Xi’an 710021,China) |
| |
| Abstract: | Bi2Ti2O7 thin film was prepared on the glass substrate by the self-assembled monolayer(SAM) tech-nique with Bi(NO3)3 and Ti(OC4H9)4 as the raw materials and octadecyltrichlorosilane as the template.The crystal phase composition,microstructure and topography of the Bi2Ti2O7 thin films were characterized by various techniques,including X-ray diffraction,field-emission scanning electron microscopy,energy disperse spectroscopy and atomic force microscopy.The results indicate the pure cubic phase Bi2Ti2O7 thin film is successfully prepared after annealing at 540℃ for 2h.The prepared Bi2Ti2O7 thin film has a flat,homogeneous and dense surface. |
| |
| Keywords: | self-assembled monolayer Bi2Ti2O7 thin film characterization |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
